高等学校化学学报 ›› 1995, Vol. 16 ›› Issue (4): 568.

• 论文 • 上一篇    下一篇

O-烷基苯基硫代膦酰取代硫脲的合成(Ⅲ)──含P─C键化合物的研究

胡式贤, 张继才, 丁言伟, 赵洪刚   

  1. 辽宁师范大学化学系, 大连, 116022
  • 收稿日期:1994-04-27 出版日期:1995-04-24 发布日期:1995-04-24
  • 通讯作者: 胡式贤,男,51岁,博士,副教授.
  • 作者简介:胡式贤,男,51岁,博士,副教授.
  • 基金资助:

    辽宁省教育委员会重点学科基金

Synthesis of O-Alkylphenylthioureidophosphonothioates──A Study of the Compounds Including P-C Bonds

HU Shi-Xian, ZHANG Ji-Cai, DING Yan-Wei, ZHAO Hong-Gang   

  1. Department of Chemistry, Liaoning Normal University, Dalian, 116022
  • Received:1994-04-27 Online:1995-04-24 Published:1995-04-24

摘要: 利用O-烷基苯基硫代膦酸异硫氰基酯与胺的加成反应,合成了两系列O-烷基苯基硫代膦酰取代硫腺化合物。经元素分析、IR和1NNMR确定了它们的结构,并进行了除草活性的测试。

关键词: 硫代膦酰取代硫脲, 除草活性, 合成

Abstract: By the reactions of O-alkylphenylthiocyanatidophosphonothioates with amines,two series of O-alkylphenylthioureidophosphonothioates were prepared.The structures of these compounds have been confirmed by IR, NMR and elementary analysis.The results from the biossay show that these compounds have no significant herbicidal activity.

Key words: O-Alkylphenylthioureidophosphonothioate, Herbicidal activity, Synthesis

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