高等学校化学学报

高等学校化学学报 ›› 1992, Vol. 13 ›› Issue (3): 332.

• 论文 • 上一篇    下一篇

三苯基锡-O,O-二芳基二硫代磷酸酯的合成和结构表征

李靖, 谢庆兰, 罗宁, 张殿坤, 贺水济   

  1. 南开大学元素有机化学研究所, 天津, 300071
  • 收稿日期:1991-04-20 出版日期:1992-03-24 发布日期:1992-03-24
  • 通讯作者: 谢庆兰
  • 基金资助:

    天津二十一世纪青年科学基金

Synthesis and Spectra Analysis of Triphenyltin-O,O- Diaryl dithiophosphates

LI Jing, XIE Qing-lan, LUO Ning, ZHANG Dian-kun, HE Shui-ji   

  1. Institute of Elemento-Organic Chemistry, Nankai University, Tianjin, 300071
  • Received:1991-04-20 Online:1992-03-24 Published:1992-03-24

PDF (PC)

被引次数

4

摘要： 本文合成了13种三苯基锡-O,O-二芳基二硫代磷酸酯,测定了它们的IR、1H、31C、119SnNMR,MS和元素分析,结果表明该类化合物具有单体的四面体四价锡结构。

关键词: 三苯基锡, 二硫代磷酸酯, 合成, 波谱

Abstract: Triphenyltin-O, O-diaryldithiophosphates derivatives are a kind of organotin compounds with high biological activities.In this paper 13 triphenyltin-O, O-diaryldithiophosphates were synthesized.The IR, 1H NMR, 13C NMR, 119Sn NMR, MS and elemental analysis were determined.These results show that the structures of all compounds contain a four-coordinate tin atom.

Key words: Triphenyltin, Dithiophosphates, Synthesis, Spectra analysis

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