高等学校化学学报

高等学校化学学报 ›› 1989, Vol. 10 ›› Issue (6): 655.

• 研究简报 • 上一篇    下一篇

1.3.2-二氮磷杂环戊烷类化合物的合成

陈茹玉, 刘准, 李晨曦   

  1. 南开大学元素有机化学研究所
  • 收稿日期:1987-12-11 出版日期:1989-06-24 发布日期:1989-06-24
  • 通讯作者: 陈茹玉
  • 基金资助:

    国家自然科学基金

Synthesis of 1,3,2-Diazaphospholidines

Chen Ruyu, Liu Zhun, Li Chenxi   

  1. Researeh Institute of Elemento Organic Chemistry, Nankai University, Tianjin
  • Received:1987-12-11 Online:1989-06-24 Published:1989-06-24

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摘要： 为了寻找新的除草剂,我们研究了N,N′-二取代苯磺酰乙二胺与不同类型磷化合物的反应(这里有图片19890623-655-3.gif)。

关键词: 1, 3, 2-二氮磷杂环戊烷, 合成, NMR谱, MS谱

Abstract: The reactions of N, N' -bis (substituted benzenesulfonyl) ethylenedi-amine with phosphites and hexaalkyl phosphorous amides were studied. It was found that N,N'-bis(substituted benzenesulfonyl)ethylenediamine could not react with phosphites, but could do with phosphorous amides to form 1,3,2-diazaphos-pholidines. NMRand MSspectra of 1,3,2-diazaphospholidines were discussed.

Key words: 1,3,2-Diazaphospholidine, Synthesis, NMR Spectra, MS. Spectra

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