高等学校化学学报

高等学校化学学报 ›› 2001, Vol. 22 ›› Issue (8): 1290.

• 研究快报 • 上一篇    下一篇

一个新型层状化合物[Ni(C10H8N2)2V3O8.5]的水热合成与晶体结构

栾国有1, 王恩波1, 韩正波1, 李阳光1, 鹿颖1, 胡长文1, 胡宁海2, 贾恒庆2   

  1. 1. 东北师范大学化学学院, 长春 130024;
    2. 长春应用化学研究所, 长春 130022
  • 收稿日期:2001-04-09 出版日期:2001-08-24 发布日期:2001-08-24
  • 通讯作者: 王恩波(1936年出生),男,教授,博士生导师,从事多金属氧酸盐材料研究.
  • 基金资助:

    国家自然科学基金(批准号:29771006)

Hydrothermal Synthesis and Crystal Structure of a Novel Layered Compound [Ni(C10H8N2)2V3O8.5]

LUAN Guo-You1, WANG En-Bo1, HAN Zheng-Bo1, LI Yang-Guang-LU Ying1, HU Chang-Wen1, HU Ning-Hai1, JIA Heng-Qing2   

  1. 1. Department of Chemistry, Northeast Normal University, Chang chun 130024, China;
    2. Chang chun Institute of Applied Chemistry, Academia Sinica, Chang chun 130022, China
  • Received:2001-04-09 Online:2001-08-24 Published:2001-08-24

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关键词: 水热合成, 层状化合物, 晶体结构

Abstract: Anovel layered compound, [Ni(C10 H8N2)2V3O8.5], was hydrothermally synthesized and structurally characterized by single crystal X-ray diffraction. The compound crystallizes in monoclinic system, space group P21/c with a=15518(3)nm, b=14761(3)nm, c=10483(2)nm, β=9202(3)°, V=23998 (8)nm3, Z=4, R=00467, wR2=00859.

Key words: Hydrothermal synthesis, Layered compound, Crystal structure

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