Chem. J. Chinese Universities ›› 2014, Vol. 35 ›› Issue (8): 1629.doi: 10.7503/cjcu20131282
• Articles: Inorganic Chemistry • Previous Articles Next Articles
KUANG Daizhi*(), FENG Yonglan, YU Jiangxi, ZHANG Fuxing, JIANG Wujiu, PENG Yan, ZHU Xiaoming, TAN Yuxing
Received:
2013-12-27
Online:
2014-08-10
Published:
2014-07-04
Contact:
KUANG Daizhi
E-mail:hnkcq@qq.com
Supported by:
CLC Number:
TrendMD:
KUANG Daizhi, FENG Yonglan, YU Jiangxi, ZHANG Fuxing, JIANG Wujiu, PENG Yan, ZHU Xiaoming, TAN Yuxing. Microwave Assisted Solid-state Synthesis, Crystal Structure, Properties of the Coordination Polymer Constructed from Tricyclohexyltin Hydroxide and o-Ferrocenylcarbonyl Benzoic Acid†[J]. Chem. J. Chinese Universities, 2014, 35(8): 1629.
Sn1—C1 | 0.2155(4) | Sn1—C7 | 0.2146(4) | Sn1—C13 | 0.2159(4) |
---|---|---|---|---|---|
Sn1—O1# | 0.2126(2) | Sn1—O3 | 0.2651 | ||
O1#—Sn1—C1 | 96.69(15) | O1#—Sn1—C7 | 104.70(12) | O1#—Sn1—C13 | 92.09(14) |
C7—Sn1—C1 | 124.06(17) | C1—Sn1—C13 | 116.48(19) | C7—Sn1—C13 | 113.69(17) |
O3—Sn1—C1 | 82.45 | O3—Sn1—C7 | 83.35 | O3—Sn1—C13 | 79.98 |
O1#—Sn1—O3 | 170.53 |
Table 1 Selected bond lengths(nm) and bond angles(°) of the complex*
Sn1—C1 | 0.2155(4) | Sn1—C7 | 0.2146(4) | Sn1—C13 | 0.2159(4) |
---|---|---|---|---|---|
Sn1—O1# | 0.2126(2) | Sn1—O3 | 0.2651 | ||
O1#—Sn1—C1 | 96.69(15) | O1#—Sn1—C7 | 104.70(12) | O1#—Sn1—C13 | 92.09(14) |
C7—Sn1—C1 | 124.06(17) | C1—Sn1—C13 | 116.48(19) | C7—Sn1—C13 | 113.69(17) |
O3—Sn1—C1 | 82.45 | O3—Sn1—C7 | 83.35 | O3—Sn1—C13 | 79.98 |
O1#—Sn1—O3 | 170.53 |
Fig.3 2D supramolecular structure of the complex by C—H…π interactions C34#—H34#…π(C20—C25) 0.3555 nm, #: 1-x, 1-y, -z. Cyclohexyl groups are omitted for clarity.
Sample | IC50/(μmol·L-1) | ||||
---|---|---|---|---|---|
HepG2 | KB | MCF-7 | A549 | HT-29 | |
Complex | 0.298 | 0.935 | 0.293 | 1.008 | 0.079 |
cis-Platin | 65.32 | 2.650 | 88.17 | 1.510 | 58.06 |
Table 2 IC50 values of the complex and cis-platin on HepG2, KB, MCF-7, A549 and HT-29
Sample | IC50/(μmol·L-1) | ||||
---|---|---|---|---|---|
HepG2 | KB | MCF-7 | A549 | HT-29 | |
Complex | 0.298 | 0.935 | 0.293 | 1.008 | 0.079 |
cis-Platin | 65.32 | 2.650 | 88.17 | 1.510 | 58.06 |
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