高等学校化学学报 ›› 2002, Vol. 23 ›› Issue (6): 1002.

• 研究快报 • 上一篇    下一篇

新型三维H0.5CoP0.5O2.5的水热合成与结构表征

李传碧1, 徐吉庆1, 曾庆新1, 苏畅1, 张丽娟1, 叶铃2   

  1. 1. 吉林大学化学学院;
    2. 吉林大学超分子结构与光谱实验室, 长春 130023
  • 收稿日期:2001-08-30 出版日期:2002-06-24 发布日期:2002-06-24
  • 通讯作者: 徐吉庆(1937年出生),男,教授,博士生导师,从事簇合物功能材料研究.
  • 基金资助:

    国家自然科学基金(批准号:29733090);高等学校博士学科点专项基金资助

Hydrothermal Synthesis and Crystal Structure of a Novel 3-D Compound [H0.5CoP0.5O2.5]

LI Chuan-Bi1, XU Ji-Qing1, ZENG Qing-Xin1, SU Chang1, ZHANG Li-Juan1, YE Ling2   

  1. 1. College of Chemistry, Jilin University, Changchun 130023, China;
    2. Key Laboratory of Superamolecular Structure and Spectroscopy, Jilin University, Changchun 130023, China
  • Received:2001-08-30 Online:2002-06-24 Published:2002-06-24

关键词: 水热合成, 三维化合物, 晶体结构

Abstract: Anovel 3-D compound, [H0.5CoP0.5 O2.5], was hydrothermally synthesized and structurally characterized by singly crystal X-ray diffraction, ICP, elemental analysis and IRspectra. The compound crystallizes in orthorhombic system, space group Pnnm with a=0.8051(2) nm, b=0.83809(13) nm, c=0.5950(2) nm, V=0.401(2) nm3, Z=1, D=1.669 Mg/cm3, R=0.0491, wR=0.1532.

Key words: Hydrothermal synthesis, 3-Dimension compound, Crystal structure

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