高等学校化学学报

高等学校化学学报 ›› 1995, Vol. 16 ›› Issue (11): 1718.

• 论文 • 上一篇    下一篇

酰氨基硫脲及相关杂环衍生物研究(XXV)──1-[5′-氨基-1′-(4″-氯苯基)-1′,2′,3′-三唑-4′-甲酰基]-4-芳基氨基硫脲的合成和波谱研究

张自义1, 董恒山1, 杨世琰2, 陈茂齐2   

  1. 1. 兰州大学化学系, 应用有机化学国家重点实验室, 兰州, 730000;
    2. 中国科学院兰州化学物理研究所
  • 收稿日期:1994-11-06 修回日期:1995-05-17 出版日期:1995-11-24 发布日期:1995-11-24
  • 通讯作者: 张自义,男,61岁,教授.
  • 作者简介:张自义,男,61岁,教授.

Studies on Acylthiosemicarbazides and Related Heterocyclic Derivatives (XXV)──Synthetic and Spectroscopic Studies on1-[5′-Amino-1′- (4′-chloropbenyl)-1′,2′,3′-triazol-4′-acyl]-4-arylthiosemicarbazides

ZHANG Zi-Yi1, DONG Heng-Shan1, YANG Shi-Yan2, CHEN Mao-Qi2   

  1. 1. Departnient of Chemistry, National Laboratory of Applied Organic Cheniistry, Lanzhou University, Laenzhou, 730000;
    2. Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences
  • Received:1994-11-06 Revised:1995-05-17 Online:1995-11-24 Published:1995-11-24

PDF (PC)

摘要： 通过5-氨基-1-(4′-氯苯基)-4-甲酰肼基-1,2,3-三唑与芳基异硫氰酸酯的反应,合成了13种新的1-[5′-氨基-1′-4″-氯苯基)-1′,2′,3′-三唑-4′-甲酰基]-4-芳基氨基硫脲类化合物3a-1,经元素分析、IR、1HNMR以及MS确证其结构。

关键词: 1, 2, 3-三唑, 硫脲, 杂环, 合成, 连三唑

Abstract: We prepared 13 new derivatives 3a-1,of 1-[5′-amino-1′-(4′- chlorophenyl)-1′,2′,3 ′- triazol-4 ′- acyl]-4-arylthiosemicarbazides by reaction of 5-amino-1-(4 ′-chlorophenyl)-4-carbohydrazide-1,2,3-triazole with several arylisothiocyanates; The structures of all compounds were confirmed by elemental analysis, IR,1HNMR and MS.

Key words: Triazole, Thiosemicarbazides, Heterocycle, Synthesis, V-triazole

TrendMD: