Preparation and Characterization of Ordered Mesoporous Alumina with High Specific Surface Area with F127 as Template

Chem. J. Chinese Universities

• 研究论文 • Previous Articles Next Articles

Preparation and Characterization of Ordered Mesoporous Alumina with High Specific Surface Area with F127 as Template

LI Zhi-Ping¹, ZHAO Rui-Hong², GUO Fen¹*, CHEN Jian-Feng¹, WANG Gang¹

1. Key Lab for Advanced Preparation Technology and Application with of Nanomaterials, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, China;
2. School of Chemistry and Pharmaceutical Engineering, Hebei University of Science and Technology, Shijiazhuang 050018, China

Received:2007-06-24 Revised:1900-01-01 Online:2008-01-10 Published:2008-01-10
Contact: GUO Fen

Abstract

Abstract: Ordered mesoporous alumina was synthesized by sol-gel method with isopropoxide alumina as the source of alumina and PEO-PPO-PEO block copolymer F127 as the template. The results show that the mesoporous alumina surface area(480 m²/g), narrow pore size distribution(2—20 nm), and lange pore volume(over 1.2 cm³/g). Worm-like pore was formed and ordered to some extent. The structure of the synthesized sample was investigated by BET, TEM, and XRD technologies. The influence of various conditions on the structure of ordered mesoporous alumina was discussed.

Key words: PEO-PPO-PEO block copolymer F127, Ordered mesoporous alumina, High specific surface aera

CLC Number:

O614.3

TrendMD:

LI Zhi-Ping¹, ZHAO Rui-Hong², GUO Fen¹*, CHEN Jian-Feng¹, WANG Gang¹. Preparation and Characterization of Ordered Mesoporous Alumina with High Specific Surface Area with F127 as Template[J]. Chem. J. Chinese Universities, doi: .

References

Related Articles 15

[1]	LU Cong, LI Zhenhua, LIU Jinlu, HUA Jia, LI Guanghua, SHI Zhan, FENG Shouhua. Synthesis， Structure and Fluorescence Detection Properties of a New Lanthanide Metal-Organic Framework Material [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220037.
[2]	HAN Zongsu, YU Xiaoyong, MIN Hui, SHI Wei, CHENG Peng. A Rare Earth Metal-Organic Framework with H₆TTAB Ligand [J]. Chem. J. Chinese Universities, 2022, 43(1): 20210342.
[3]	LIU Xueguang, YANG Xiaoshan, MA Jingjing, LIU Weisheng. Separating Methyl Blue Selectively from the Mixture of Dyes by Europium Metal-organic Frameworks [J]. Chem. J. Chinese Universities, 2022, 43(1): 20210715.
[4]	HUANG Wenjuan, HOU Huayi, CHEN Xiangbai, ZHAI Tianyou. Synthesis of InSe Nanoflakes with Near-infrared Photoresponse Grown by Chemical Vapor Deposition ^† [J]. Chem. J. Chinese Universities, 2020, 41(4): 682.
[5]	WANG Pengcheng, SHAN Liang, FAN Yong, WANG Li, XU Jianing, WU Shujie. Syntheses of MIL-53 MOFs Materials and Their Catalytic Properties in Strecker Reactions [J]. Chem. J. Chinese Universities, 2019, 40(8): 1655.
[6]	ZHAO Yuxuan,CHEN Yanjun,PAN Guxin,WANG Chang,PENG Zhenbo,SUN Zongxu,LIANG Yongri,SHI Qisong. Preparation and Performance of Novel Tb-PEG+Eu-PEG/PANI/PAN Luminescent-electrical-phase Change Composite Fibers by Electrospinning^† [J]. Chem. J. Chinese Universities, 2019, 40(4): 824.
[7]	FU Linjie,LUO Ran,WANG Shuhua,ZHANG Ning,CHEN Chao. Synthesis of Novel Cd(Ⅱ) Metal-organic Framework for Highly Selective Detection of p-Nitroaniline^† [J]. Chem. J. Chinese Universities, 2019, 40(3): 419.
[8]	ZHANG Chunyan,LUO Jianxin,LI Wenjun,OU Lijuan,YU Guipeng,PAN Chunyue. Preparation and Sensing Properties of Covalent-linked Europium Complex Monodisperse Polystyrene Microspheres^† [J]. Chem. J. Chinese Universities, 2019, 40(1): 153.
[9]	LI Jian,XIE Linxia,LIANG Zupei,GUO Rong,LIU Chenyu,MA Shulan. Luminescence Property and Detection Capability Towards Hg²⁺ of LEuH Composites with Mo $S 4 2 -$ and OS^- Anions^† [J]. Chem. J. Chinese Universities, 2018, 39(10): 2154.
[10]	TANG Keyun,LI Luoyuan,FU Limin,AI Xicheng,ZHANG Jianping. Effect of Crystal Matrix on Energy Transfer Mechanism in Rare-earth Upconversion Nanomaterials^† [J]. Chem. J. Chinese Universities, 2018, 39(10): 2136.
[11]	WANG Caiping, LI Youfen, ZHANG Yidong. Preparation of Glass Ceramics Containing CaF₂ by One-step Method and Analysis of the Fluorescent Probe of Eu³⁺ Ion^† [J]. Chem. J. Chinese Universities, 2016, 37(4): 607.
[12]	KANG Xiaoyan, HE Anqi, WANG Jingdan, GUO Ran, ZHAI Yanjun, XU Yizhuang, WU Jinguang. Investigation on the Enrichment of DNA Using Lanthanum Carbonate^† [J]. Chem. J. Chinese Universities, 2016, 37(1): 7.
[13]	YANG Shuilan, SONG Pan, SHE Wenjie, YANG Tianlin. Mechanism of the Interaction Between a Phosphorus-containing Tripod Ligand Europium(Ⅲ) Complex and Bovine Serum Albumin^† [J]. Chem. J. Chinese Universities, 2015, 36(7): 1254.
[14]	WEN Jinyan, LÜ Biaobiao, ZHANG Yang, WANG Jiamin, YING Xiao, WANG Hui, JI Liangnian, LIU Haiyang. Interaction of Human Serum Albumin and Water Soluble Cationic Pyridyl Corrole Gallium Complex^† [J]. Chem. J. Chinese Universities, 2015, 36(6): 1033.
[15]	LI Xu, JIANG Jianhong, HAN Buxing, GU Huiwen, XIE Zhaofeng, CHEN Lan, XIAO Shengxiong, LI Chuanhua, LI Aitao, LI Xia, YAO Feihong, WANG Qun, LI Qiangguo. Synthesis and Biological Activities of o-Vanillin-histidine Schiff-base and Its Lanthanum Complex^† [J]. Chem. J. Chinese Universities, 2015, 36(5): 856.

Preparation and Characterization of Ordered Mesoporous Alumina with High Specific Surface Area with F127 as Template

PDF (PC)

Knowledge

Cited

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments