Hydrothermal Synthesis and Crystal Structure of Co(En)3MoO4

Abstract

Abstract: Co(En)₃MoO₄ was synthesized by using the method of hydrothermal synthesis and characterized by elemental analysis, IR, ESRand single-crystal X-ray methods. It crystal-lizes in hexagonal space group P3C1 with a=1.5964(2) nm, b=1.5964(2) nm, c=0.9935(2) nm, α=β=90°, γ=120°, M_c=399.18, V=2.1926(6) nm³, D_c=1.814 g/nm³, Z=6, F(000)=1218, R₁=0.0703, R_w=0.2207. According to separation of anion which acted on electrostatic potential, the anion and cation ions formed a type of organic and inorganic material.

Key words: Hydrothermal synthesis, Crystal, P3C1

CLC Number:

O611

TrendMD:

WANG Ren-Zhang, LI Ya-Feng, QIAO Xiao-Guang, YANG Guo-Yu, XING Yong-Heng, ZENG Qing-Xin, XU Ji-Qing, LIN Yong-Hua, XING Yan, JIA Heng-Qing . Hydrothermal Synthesis and Crystal Structure of Co(En)₃MoO₄[J]. Chem. J. Chinese Universities, 1999, 20(8): 1186.

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Hydrothermal Synthesis and Crystal Structure of Co(En)₃MoO₄

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