Studies on Flow-injection Stopped-flow Florescence Kinetic Method for Determination of Trace Iron

Abstract

Abstract: A new flow-injection stopped-flow fluorescence kinetic method for determination of trace iron(Ⅲ) was proposed. The method is based on monitoring the binary fluorescence complex formation of Fe(Ⅲ) with 3,5-dibro mosalicylfluorone(DBSAF) at 510 nm/510 nm in an acidic medium.The linearity range is between 0.020 and 0.250 μg/mLwith a correction coefficient of 0.999 and a detection limitation of 10 ng/mL. The method has been ap plied to the determination of Fe(Ⅲ)in alluminum alloy and peach leaves, the results are in agreement with ICPmethod and standard reference value, respectively.

Key words: Flow-injection stopped-flow technique, Fluorescence kinetic anaiysis, Iron(Ⅲ), 3, 5-Dibromosalicylfluorone

TrendMD:

HUANG Hou-Ping, CAI Ru-Xiu, ZENG Yun-E, GAO Deng-Yun. Studies on Flow-injection Stopped-flow Florescence Kinetic Method for Determination of Trace Iron[J]. Chem. J. Chinese Universities, 1995, 16(1): 47.

[1]	ZHANG Qingyi, CAO Jie, SHU Xiao, LIU Jianzhao. Effects of Exogenous N⁶-methyladenosine (m⁶A) Incorporation on the Expression of Cellular mRNA Transcripts [J]. Chem. J. Chinese Universities, 2022, 43(Album-4): 20220173.
[2]	HUANG Qiuhong, LI Wenjun, LI Xin. Organocatalytic Enantioselective Mannich-type Addition of 5H-Oxazol-4-ones to Isatin Derived Ketimines [J]. Chem. J. Chinese Universities, 2022, 43(8): 20220131.
[3]	WANG Xuebin, XUE Yuan, MAO Hua’nyu, XIANG Yanxin, BAO Chunyan. Preparation of Photo/reduction Dual-responsive Hydrogel Microspheres and Their Application in Three-dimensional Cell Culture [J]. Chem. J. Chinese Universities, 2022, 43(8): 20220116.
[4]	JIN Ruiming, MU Xiaoqing, XU Yan. Bio-chemical Synthesis of Melanin Precursor—— 5，6-Dihydroxyindole（DHI） [J]. Chem. J. Chinese Universities, 2022, 43(8): 20220134.
[5]	TAN Yan, YU Shen, LYU Jiamin, LIU Zhan, SUN Minghui, CHEN Lihua, SU Baolian. Efficient Preparation of Mesoporous γ-Al₂O₃ Microspheres and Performance of Pd-loaded Catalysts [J]. Chem. J. Chinese Universities, 2022, 43(8): 20220133.
[6]	YAO Yiting, LYU Jiamin, YU Shen, LIU Zhan, LI Yu, LI Xiaoyun, SU Baolian, CHEN Lihua. Preparation of Hierarchical Microporous-mesoporous Fe₂O₃/ZSM-5 Hollow Molecular Sieve Catalytic Materials and Their Catalytic Properties for Benzylation [J]. Chem. J. Chinese Universities, 2022, 43(8): 20220090.
[7]	WANG Hong, SAN Khin Nyein Ei, FANG Yun, ZHANG Xinyu, FAN Ye. Pickering Emulsion Stabilization and Interfacial Catalytic Oxidation by Janus Nano-Au [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220105.
[8]	WANG Guangqi, BI Yiyang, WANG Jiabo, SHI Hongfei, LIU Qun, ZHANG Yu. Heterostructure Construction of Noble-metal-free Ternary Composite Ni（PO₃）₂-Ni₂P/CdS NPs and Its Visible Light Efficient Catalytic Hydrogen Production [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220050.
[9]	JIANG Xiaokang, ZHOU Qi, ZHOU Hengwei. Synthesis and Luminescence Properties of Gd₂ZnTiO₆∶Dy³⁺， Eu³⁺ Single Phase White Light-emitting Phosphors [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220029.
[10]	LIU Xiaolei, LU Yongqiang, YOU Qi, LIU Guohui, YAO Wei, HU Riming, YAN Jixian, CUI Yu, YANG Xiaofeng, SUN Guoxin, JIANG Xuchuan. A 3-Hydroxythalidomide-based Ratiometric Fluorescent Probe for the Detection of H₂O₂ [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220070.
[11]	GONG Yanxi, WANG Jianbing, CHAI Buyu, HAN Yuanchun, MA Yunfei, JIA Chaomin. Preparation of Potassium Doped g-C₃N₄ Thin Film Photoanode and Its Application in Photoelectrocatalytic Oxidation of Diclofenac Sodium in Water [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220005.
[12]	HUANG Yi, LYU Lingling, PAN Xiaopeng, SUN Guangdong, LI Yongqiang, YAO Juming, SHAO Jianzhong. Three-dimensional Printing of Photocrosslinked Self-supporting Silk Fibroin Hydrogels [J]. Chem. J. Chinese Universities, 2022, 43(4): 20210841.
[13]	ZHAO Mengyang, HUANG Ziyang. Preparation and in vitro Bioactivity of HA/CuO/SrCO₃ Gradiently Composite Coating [J]. Chem. J. Chinese Universities, 2022, 43(2): 20210644.
[14]	ZHANG Zhibo, SHANG Han, XU Wenxuan, HAN Guangdong, CUI Jinsheng, YANG Haoran, LI Ruixin, ZHANG Shenghui, XU Huan. Self-Assembly of Graphene Oxide at Poly（3-hydroxybutyrate） Microparticles Toward High-performance Intercalated Nanocomposites [J]. Chem. J. Chinese Universities, 2022, 43(2): 20210566.
[15]	ZHANG Zhinan, CHENG Haiming, TENG Shiyong, ZHANG Ying. Synthesis and Optical Properties of RbPb₂Cl₅ [J]. Chem. J. Chinese Universities, 2022, 43(11): 20220418.

Studies on Flow-injection Stopped-flow Florescence Kinetic Method for Determination of Trace Iron

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments