高等学校化学学报 ›› 2005, Vol. 26 ›› Issue (10): 1795.

• 研究简报 • 上一篇    下一篇

水热微乳法合成La(OH)3纳米棒的形貌控制研究

尹贻东1,2,3, 洪广言1   

  1. 1. 中国科学院长春应用化学研究所,稀土化学与物理重点实验室,长春130022
    2. 黑龙江大学化学化工及材料学院,哈尔滨150080;
    3. 中国科学院研究生院,北京100049
  • 收稿日期:2005-05-11 出版日期:2005-10-10 发布日期:2005-10-10
  • 基金资助:

    国家自然科学基金(批准号:20071031)资助.

Morphology Control of Lanthanum Hydroxide Nanorods Synthesized by Hydrothermal Microemulsion Method

YIN Yi-Dong1,2,3, HONG Guang-Yan1   

  1. 1. Key Laboratory of Rare Earth Chemistry and Physics,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022,China;
    2. School of Chemistry and Materials Science,Heilongjiang University,Harbin 150080,China;
    3. Graduate School of the Chinese Academy of Sciences,Beijing 100049,China
  • Received:2005-05-11 Online:2005-10-10 Published:2005-10-10

关键词: 稀土, 纳米棒, 水热微乳, La(OH)3

Abstract: Lanthanum hydroxide nanorods with a diameter of 10-20 nm and length up to 100-200 nm were synthesized through a direct reaction of La(NO3)3 and KOH under hydrothermal microemulsion conditions.X-ray diffraction(XRD) and scanning electron microscope(SEM) were employed for the characterization of the structure,compositions and morphology of the obtained products.The results showed that the molar ratio of water to the surfactant CTAB,concentration of La(NO3)3,reactant temperature and reactant time all could affect the morphology and size of the lanthanum hydroxide nanorods.

Key words: Rare earth, Nanorods, Hydrothermal microemulsion, Lanthanum hydroxide

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