高等学校化学学报

高等学校化学学报 ›› 1991, Vol. 12 ›› Issue (9): 1204.

• 论文 • 上一篇    下一篇

四苯基苯基五苯基苯基二乙氧基硅烷的分离制备和鉴定

王吉顺1, 关家锐1, 陈剑华2, 张晓菁2   

  1. 1. 山东大学实验中心, 济南, 250100;
    2. 山东大学新材料研究所
  • 收稿日期:1990-05-29 出版日期:1991-09-24 发布日期:1991-09-24
  • 通讯作者: 王吉顺

Separation, Preparation and Identification of Tetraphenyl-phenylpentaphenylphenyldiethoxysilicane

Wang Ji-shun1, Guan Jia-rui1, Chen Jian-hua2, Zhang Xiao-jing2   

  1. 1. Experimental Center, Shandong University, Jinan, 250100;
    2. New Material Institute, Shandong University, Jinan
  • Received:1990-05-29 Online:1991-09-24 Published:1991-09-24

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摘要： 杜作栋等先后合成了四苯基苯基有机硅化合物和五苯基苯基有机硅化合物,并用溶剂沉淀法和重结晶法纯化产物后进行结构分析,在此基础上陈剑华等又合成了双多苯基苯基有机硅化合物,此类化合物具有更好的耐高温性能,可制成耐高温树脂、耐高温橡胶、耐高温粘合剂和耐高温涂料。

关键词: 四苯基苯基五苯基苯基二乙氧基硅烷, 分离, 制备, 高效液相色谱, 质谱

Abstract: The paper reports the separation and preparation of tetraphenylphenylpentaphenyl-phenyldiethoxysilicane by HPLC. The structure of compound is identified by 1R, NMR and MS. The by-products in the synthetic process were also analysed and discussed.

Key words: Tetraphenylphenylpentaphenylphenyldiethoxysilicane, Separation, Preparation, HPLC, MS

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