Chem. J. Chinese Universities ›› 2014, Vol. 35 ›› Issue (9): 1968.doi: 10.7503/cjcu20140205
• Physical Chemistry • Previous Articles Next Articles
HUANG Jianye, WANG Fenghui*(), HOU Shaohang, ZHAO Xiang
Received:
2014-03-11
Online:
2014-09-10
Published:
2019-08-01
Contact:
WANG Fenghui
E-mail:fhwang@nwpu.edu.cn
Supported by:
CLC Number:
TrendMD:
HUANG Jianye, WANG Fenghui, HOU Shaohang, ZHAO Xiang. Fabrication of Superhydrophobic Surfaces with Hierarchical Structures by an Ultrasonic Etch Method†[J]. Chem. J. Chinese Universities, 2014, 35(9): 1968.
Fig.2 SEM images of steel surfaces after ultrasonic etch (A1, A2) 60Si2Mn; (B1, B2) 60#; (C1, C2) T10; (D1, D2) Cr06. Insets in (A1—D1): micro-photographs of contact angle(CA).
Fig.3 SEM images of 65Mn surfaces after etch(A1, A2, B1, B2) and micro-photographs of water contact angles(A3, B3) (A1—A3) Regular etch; (B1—B3) ultrasonic etch. Inside the ellipses show the second-phase particles.
Fig.4 SEM images of silicon surfaces after etch(A1, A2, B1, B2) and micro-photographs of water contact angles(A3, B3) (A1—A3) Regular etch; (B1—B3) ultrasonic etch.
Fig.5 SEM images of pure iron surfaces after etch(A1, A2, B1, B2) and micro-photographs of water contact angles(A3, B3) (A1—A3) Regular etch; (B1—B3) ultrasonic etch.
Specimen | Etch method | Microstructure | Size/μm | Nanostructure | Size/nm | Contact angle/(°) | Roll angle/(°) |
---|---|---|---|---|---|---|---|
60Si2Mn | Ultrasonic | Bump & ridge | 1—5 | Particles | 50—100 | 157.0 | 6.5 |
60# | Ultrasonic | Rice straw | 0.5—5 | Particles | 50—150 | 155.8 | 19.2 |
T10 | Ultrasonic | Ball cactus | 1—3 | Flakiness | 50—700 | 157.4 | 6.1 |
Cr06 | Ultrasonic | Bump & cavity | 0.5—5 | Particles | 30—120 | 154.9 | 7.8 |
65Mn | Regular | Bump & ridge | 2—10 | 126.8 | 180 | ||
65Mn | Ultrasonic | Bump & valley | 1—5 | Flakiness | 50—300 | 157.6 | 6.7 |
Silicon steel | Regular | 119.2 | 180 | ||||
Silicon steel | Ultrasonic | Spindrift | 5—50 | Particles & flakiness | 100—500 | 156.8 | 7.2 |
Pure iron | Regular | 126.7 | 180 | ||||
Pure iron | Ultrasonic | Cavity & valley | 10—100 | Particles | 200—500 | 131.0 | 180 |
Table 1 Micro morphologies and hydrophobicity of specimen
Specimen | Etch method | Microstructure | Size/μm | Nanostructure | Size/nm | Contact angle/(°) | Roll angle/(°) |
---|---|---|---|---|---|---|---|
60Si2Mn | Ultrasonic | Bump & ridge | 1—5 | Particles | 50—100 | 157.0 | 6.5 |
60# | Ultrasonic | Rice straw | 0.5—5 | Particles | 50—150 | 155.8 | 19.2 |
T10 | Ultrasonic | Ball cactus | 1—3 | Flakiness | 50—700 | 157.4 | 6.1 |
Cr06 | Ultrasonic | Bump & cavity | 0.5—5 | Particles | 30—120 | 154.9 | 7.8 |
65Mn | Regular | Bump & ridge | 2—10 | 126.8 | 180 | ||
65Mn | Ultrasonic | Bump & valley | 1—5 | Flakiness | 50—300 | 157.6 | 6.7 |
Silicon steel | Regular | 119.2 | 180 | ||||
Silicon steel | Ultrasonic | Spindrift | 5—50 | Particles & flakiness | 100—500 | 156.8 | 7.2 |
Pure iron | Regular | 126.7 | 180 | ||||
Pure iron | Ultrasonic | Cavity & valley | 10—100 | Particles | 200—500 | 131.0 | 180 |
[1] | Feng L., Li S. H., Li Y. S., Li H. J., Zhang L. J., Zhai J., Song Y. L., Liu N.Q., Jiang L., Zhu D. B., Adv. Mater., 2002, 14(24), 1857—1860 |
[2] | Patankar N. A., Langmuir, 2004, 20(19), 8209—8213 |
[3] | Wang S. T., Jiang L., Adv. Mater., 2007, 19(21), 3423—3424 |
[4] | Neinhuis C., Barthlott W., Ann. Botany., 1997, 79(6), 667—677 |
[5] | Du C. G., Xia F., Wang S. T., Wang J. X., Song Y. L., Jiang L., Chem. J. Chinese Universities,2010, 31(3), 421—431 |
(杜晨光, 夏帆, 王树涛, 王京霞, 宋延林, 江雷. 高等学校化学学报, 2010, 31(3), 421—431) | |
[6] | Yan Y. Y., Gao N., Barthlott W., Adv. Colloid Interface Sci., 2011, 169(2), 80—105 |
[7] | Lian F., Zhang H. C., Pang L.Y., Chem. J. Chinese Universities,2011, 32(12), 2833—2837 |
(连峰, 张会臣, 庞连云. 高等学校化学学报, 2011, 32(12), 2833—2837) | |
[8] | Wen M. X., Zheng Y. M., Chem. J. Chinese Universities,2014, 35(5), 1011—1015 |
(文孟喜, 郑咏梅. 高等学校化学学报, 2014, 35(5), 1011—1015 | |
[9] | Liang X. W., Zhang Y. B., Wang B., Guo Z. G., Li W. M., Acta Chim. Sinica,2012, 70(23), 2393—2403 |
(梁欣伟, 张亚斌, 王奔, 郭志光, 李维民. 化学学报, 2012, 70(23), 2393—2403) | |
[10] | Xue C. H., Ma J. Z., J. Mater. Chem. A,2013, 1(13), 4146—4161 |
[11] | Bhushan B., Jung Y. C., Prog. Mater. Sci., 2011, 56, 1—108 |
[12] | Huang J. Y., Wang F. H., Zhao X., Zhang K., Acta Phys. -Chim. Sin., 2013, 29(11), 2459—2464 |
(黄建业, 王峰会, 赵翔, 张凯. 物理化学学报, 2013, 29(11), 2459—2464) | |
[13] | Marmur A., Langmuir, 2008, 24(14), 7573—7579 |
[14] | Lichao G., McCarthy T. J., Langmuir,2006, 22(14), 6234—6237 |
[15] | Azimi G., Dhiman R., Kwon H. M., Paxson A. T., Varanasi K. K., Nat. Mater., 2013, 12, 315—320 |
[16] | Tian Y., Jiang L., Nat. Mater., 2013, 12, 291—292 |
[17] | Lau K. K. S., Bico J., Teo K. B. K., Chhowalla M., Amaratunga G. A. J., Milne W. I., McKinley G. H., Gleason K. K., Nano Lett., 2003, 3(12), 1701—1705 |
[18] | Shiu J., Kuo C., Chen P., Mou C., Chem. Mater., 2004, 16(4), 561—564 |
[19] | Khorasani M. T., Mirzadeh H., Kermani Z., Appl. Surf. Sci., 2005, 242(3), 339—345 |
[20] | Xu W. J., Song J. L., Sun J., Lu Y., J. Chin. Ceram. Soc., 2011, 39(11), 1857—1861 |
(徐文骥, 宋金龙, 孙晶, 陆遥. 硅酸盐学报, 2011, 39(11), 1857—1861) | |
[21] | Guo Z. G., Zhou F., Hao J. C., Liu W. M., J. Am. Chem. Soc., 2005, 127(45), 15670—15671 |
[22] | Guo Z. G., Zhou F., Liu W. M., Acta Chim. Sinica,2006, 64(8), 761—766 |
(郭志光, 周峰, 刘维民. 化学学报, 2006, 64(8), 761—766) | |
[23] | Shirtcliffe N. J., McHale G., Newton M. I., Chabrol G., Perry C. C., Adv. Mater., 2004, 16(21), 1929—1932 |
[24] | Jin M. H., Liao M. Y., Zhai J., Jiang L., Acta Chim. Sinica,2008, 66(1), 145—148 |
(金美花, 廖明义, 翟锦, 江雷. 化学学报, 2008, 66(1), 145—148) | |
[25] | Zhai L., Cebeci F. C., Cohen R. E., Rubner M. F., Nano Lett., 2004, 4(7), 1349—1353 |
[26] | Qian B. T., Shen Z. Q., Langmuir,2005, 21(20), 9007—9009 |
[27] | Wang Q., Zhang B.W., Qu M. N., Zhang J. Y., He D. Y., Appl. Surf. Sci., 2008, 254, 2009—2012 |
[28] | Ashokkumar M., Ultrason Sonochem., 2011, 18(4), 864—872 |
[29] | Ashokkumar M., Lee J., Kentish J., Grieser F., Ultrason Sonochem., 2007, 14(4), 470—475 |
[30] | Cassie A. B. D., Baxter S., Trans. Faraday Soc., 1944, 40, 546—550 |
[31] | Bhushan B., Nosonovsky M., Jung Y. C., J. R. Soc. Interface,2007, 4(15), 643—648 |
[32] | Extrand C. W., Langmuir, 2004, 20(12), 5013—5018 |
[33] | Wenzel R. N., Ind. Eng. Chem., 1936, 28, 988—994 |
[1] | SHI Naike, ZHANG Ya, SANSON Andrea, WANG Lei, CHEN Jun. Uniaxial Negative Thermal Expansion and Mechanism in Zn(NCN) [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220124. |
[2] | CHEN Weiqin, LYU Jiamin, YU Shen, LIU Zhan, LI Xiaoyun, CHEN Lihua, SU Baolian. Preparation of Organic Hybrid Mesoporous Beta Zeolite for Alkylation of Mesitylene with Benzyl Alcohol [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220086. |
[3] | ZHANG Lingyu, ZHANG Jilong, QU Zexing. Dynamics Study of Intramolecular Vibrational Energy Redistribution in RDX Molecule [J]. Chem. J. Chinese Universities, 2022, 43(10): 20220393. |
[4] | ZENG Yonghui, YAN Tianying. Vibrational Density of States Analysis of Proton Hydration Structure [J]. Chem. J. Chinese Universities, 2021, 42(6): 1855. |
[5] | FAN Juanjuan, HAN Yuanyuan, CUI Jie. Monte Carlo Simulation of the Transformation Control of ABC Triblock Copolymer Micelles from Multicompartment Structure to Multicore Structure [J]. Chem. J. Chinese Universities, 2021, 42(3): 857. |
[6] | WANG Yuyao, ZHANG Qiang, YU Jihong. Synthesis of Hierarchical NaX Zeolite and Its CO2 Adsorption Performance † [J]. Chem. J. Chinese Universities, 2020, 41(4): 616. |
[7] | GAO Qilong, LIANG Erjun, XING Xianran, CHEN Jun. Negative Thermal Expansion in Prussian Blue Analogues [J]. Chem. J. Chinese Universities, 2020, 41(3): 388. |
[8] | BAI Xu, HAN Chaoying, ZHU Hua. Theoretical Studies of the Potential Energy Surface and Rovibrational Spectra for Kr-C2H2 [J]. Chem. J. Chinese Universities, 2019, 40(8): 1649. |
[9] | JI Yuchun,MAO Wenhui,LIAO Hejie,WANG Jilin,LONG Fei,GU Yunle. Boron Nitride Nanotube-nanosheet Hierarchical Structures andIts Optical/adsorption Properties† [J]. Chem. J. Chinese Universities, 2019, 40(2): 216. |
[10] | LIN Dan, CHENG Min, DU Yikui, ZHU Qihe. Photofragment Translational Spectroscopy of CF3I at 238 nm:Vibrational Distribution of CF3 Fragments andCurve Crossing Probability† [J]. Chem. J. Chinese Universities, 2018, 39(8): 1713. |
[11] | CUI Yan, ZHANG Kai, CHEN Yixin, SUN Hongchen, HUANG Yang, WANG Dandan. In situ Biomimetic Remineralization of Enamel-like Hierarchical Structures† [J]. Chem. J. Chinese Universities, 2018, 39(6): 1121. |
[12] | KONG Xuelin, LU Yun, YE Guichao, LI Daohao, SUN Jin, YANG Dongjiang, YIN Yafang. Nanofibrillated Cellulose Derived Hierarchical Porous Carbon Aerogels: Efficient Anode Material for Lithium Ion Battery† [J]. Chem. J. Chinese Universities, 2017, 38(11): 1941. |
[13] | SHI Gang, BAI Huiyu, WANG Likui, SANG Xinxin, YANG Jingguo, NI Caihua, LI Ying. Fabrication of Hierarchical Hemisphere Ag Substrate Using Transfer Imprinting with No Pressure Under Ambient Temperature† [J]. Chem. J. Chinese Universities, 2017, 38(10): 1719. |
[14] |
XU Xuesong, LI Lei, JING Bo, YANG Kun.
Effect of Vibrational Excitation on the Stereodynamics of Reaction O+DCl |
[15] | ZHANG Fan, WANG Bin, WANG Jiaona, LI Xiuyan, LI Congju. Preparation of Hierarchically Structured AOPAN@Mg(OH)2 Composite Nanofibrous Membrane and Cr(Ⅵ)-removal Capacity† [J]. Chem. J. Chinese Universities, 2016, 37(11): 2117. |
Viewed | ||||||
Full text |
|
|||||
Abstract |
|
|||||