Chem. J. Chinese Universities ›› 2018, Vol. 39 ›› Issue (9): 2031.doi: 10.7503/cjcu20180110
• Physical Chemistry • Previous Articles Next Articles
HUANG Yuting, YING Zuping, ZHENG Jixing, ZHUANG Sigeng, LIU Lu, FENG Wei*()
Received:
2018-02-07
Online:
2018-09-07
Published:
2018-05-28
Contact:
FENG Wei
E-mail:weifeng@jlu.edu.cn
Supported by:
CLC Number:
TrendMD:
HUANG Yuting,YING Zuping,ZHENG Jixing,ZHUANG Sigeng,LIU Lu,FENG Wei. Hierarchical Porous ZnO Nanomaterial Synthesized with Corn Straw as Biological Templates and Its Photocatalytic Performance†[J]. Chem. J. Chinese Universities, 2018, 39(9): 2031.
Fig.7 XPS spectra of the synthesized powder(A) Wide scan survey; (B) core level spectrum for Zn2p region; (C) core level O1s spectrum, fitted with Gaussian-Lorentz distribution with Shirley type base line
Fig.8 Absorption spectra of MB dye solutions after different time irradiation(A) and the color change of methylene blue solution during irradiation(B)
Fig.9 Kinetic curves of MB(100 mL) degradation under xenon lamp irradiation(A), (B) In the presence of T-ZnO and N-ZnO, c(MB)=20 mg/L; (C), (D) in the presence of T-ZnO with different MB concentrations; (E), (F) c(MB)=20 mg/L, with different amounts of T-ZnO.
Catalyst | Synthetic method | Catalyst loading/mg | Concentration and volume | Irradiatin time/min | Degradation (%) | Ref. |
---|---|---|---|---|---|---|
ZnO nanorods | Hydrothermal method | 50 | 10 mg/L, 100 mL | 380 | 82 | [ |
ZnO | Precipitation method | 25 | 20 mg/L, 100 mL | 180 | 81 | |
ZnO | Sol-gel method | 25 | 20 mg/L, 100 mL | 180 | 92 | [ |
ZnO particles | Chemical precipitation method | 50 | 5 mg/L, 300 mL | 1103 | 97.2 | [ |
ZnO flower-like hierarchical | Hydrothermal synthesis | 50 | 10 mg/L, 60 mL | 60 | 13 | [ |
ZnO-C | Codeposition | 100 mg/L | 100 mg/L | 60 | 20 | [ |
C3N4/ZnO | Mechanical milling combined with calcination | 150 | 150 mL, 1×10-5 mol/L | 180 | 90 | [ |
ZnO nano-powder | Solution combustion synthesis | 50 | 25 mg/L, 100 mL | 120 | 86 | [ |
ZnO hierarchical porous | Bio-template | 50 | 20 mg/L, 100 mL | 180 | 98 | This work |
Table 1 Photocatalytic degradation efficiencies of ZnO nanomaterials with different morphologies toward MB dye under UV light irradiation
Catalyst | Synthetic method | Catalyst loading/mg | Concentration and volume | Irradiatin time/min | Degradation (%) | Ref. |
---|---|---|---|---|---|---|
ZnO nanorods | Hydrothermal method | 50 | 10 mg/L, 100 mL | 380 | 82 | [ |
ZnO | Precipitation method | 25 | 20 mg/L, 100 mL | 180 | 81 | |
ZnO | Sol-gel method | 25 | 20 mg/L, 100 mL | 180 | 92 | [ |
ZnO particles | Chemical precipitation method | 50 | 5 mg/L, 300 mL | 1103 | 97.2 | [ |
ZnO flower-like hierarchical | Hydrothermal synthesis | 50 | 10 mg/L, 60 mL | 60 | 13 | [ |
ZnO-C | Codeposition | 100 mg/L | 100 mg/L | 60 | 20 | [ |
C3N4/ZnO | Mechanical milling combined with calcination | 150 | 150 mL, 1×10-5 mol/L | 180 | 90 | [ |
ZnO nano-powder | Solution combustion synthesis | 50 | 25 mg/L, 100 mL | 120 | 86 | [ |
ZnO hierarchical porous | Bio-template | 50 | 20 mg/L, 100 mL | 180 | 98 | This work |
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