Chem. J. Chinese Universities ›› 2015, Vol. 36 ›› Issue (9): 1661.doi: 10.7503/cjcu20150301
• Articles: Inorganic Chemistry • Previous Articles Next Articles
HUANG Chuting, WU Xiaofeng, LI Guanghua, GAO Lu*(), FENG Shouhua
Received:
2015-04-15
Online:
2015-09-10
Published:
2015-07-24
Contact:
GAO Lu
E-mail:gaolu@jlu.edu.cn
Supported by:
CLC Number:
TrendMD:
HUANG Chuting, WU Xiaofeng, LI Guanghua, GAO Lu, FENG Shouhua. Synthesis, Structure and Luminescence Propreties of 3D Interpenetrating Metal-organic Frameworks Built by Zn(Ⅱ) and Mixed Ligands†[J]. Chem. J. Chinese Universities, 2015, 36(9): 1661.
Empirical formula | C26H16N2O8Zn2 | Z | 2 |
---|---|---|---|
Formula weight | 615.15 | Dc/(Mg·m-3) | 1.688 |
T/K | 293(2) | F(000) | 620 |
Crystal system | Monoclinic | Rint | 0.0699 |
Space group | P21/c | Goodness-of-fit on F2 | 1.106 |
a/nm | 0.64963(13) | Final R indices[I>2σ(I)] | R1=0.0518 |
b/nm | 1.7952(4) | wR2=0.1214 | |
c/nm | 1.1054(2) | R indices(all data) | R1=0.0760 |
β/(°) | 110.13(3) | wR2=0.1408 | |
V/nm3 | 1.2103(4) | Largest diff. peak and hole/(e·nm-3) | 820 , -927 |
Table 1 Crystal data and structure refinement for Zn2(BPDC)(IN)2
Empirical formula | C26H16N2O8Zn2 | Z | 2 |
---|---|---|---|
Formula weight | 615.15 | Dc/(Mg·m-3) | 1.688 |
T/K | 293(2) | F(000) | 620 |
Crystal system | Monoclinic | Rint | 0.0699 |
Space group | P21/c | Goodness-of-fit on F2 | 1.106 |
a/nm | 0.64963(13) | Final R indices[I>2σ(I)] | R1=0.0518 |
b/nm | 1.7952(4) | wR2=0.1214 | |
c/nm | 1.1054(2) | R indices(all data) | R1=0.0760 |
β/(°) | 110.13(3) | wR2=0.1408 | |
V/nm3 | 1.2103(4) | Largest diff. peak and hole/(e·nm-3) | 820 , -927 |
Fig.1 Structures of the rigid dipyridyl bridging ligand 3,6-di(pyridin-4-yl)-1,2,4,5-tetra-zine(A) and aromatic dicarboxylate ligand biphenyl-4,4'-dicarboxylic acid(B)
Fig.3 Views of the infinite two-dimensional layer constructed from dinuclear Zn2+ coordinated to IN ligands with the quadrangular channels of 1.205 nm×1.022 nm(A), the three-dimensional framework of [Zn2(BPDC)(IN)2] formed by [Zn2(—CO2)2(IN)2]∞ and BPDC ligands(B)and two-dimensional network of [Zn2(BPDC)(IN)2] with the quadrangular channels of 1.125 nm×1.462 nm(C)
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