Chem. J. Chinese Universities ›› 2011, Vol. 32 ›› Issue (3): 678.

• Articles • Previous Articles     Next Articles

Microwave-assisted Solvothermal Synthesis of Bis(nicotinate)zinc

GAO Fei, WANG  Ying, LIU Xiao-Yang*   

  1. State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry, Jilin University, Changchun 130012,  China
  • Received:2010-09-27 Revised:2010-12-08 Online:2011-03-10 Published:2011-02-23
  • Contact: Xiao-Yang LIU E-mail:liuxy@jlu.edu.cn
  • Supported by:

    国家自然科学基金(批准号: 40673051)资助.

Abstract: Bis(nicotinate)zinc was successfully synthesized under microwave-assisted solvothermal condition and the influences of reaction time, temperature, solvent, substrate concentration and heating method on the crystallization of the complexes were disscussed. With combination of the microwave-assisted solvothermal method and the conventional solvothermal method, the product so obtained not only has the advantages of microwave heating, but also has a large particle size that suitable for structural analysis.

Key words: Microwave, Solvothermal, Bis(nicotinate)zinc, Crystal

CLC Number: 

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