Chem. J. Chinese Universities ›› 2000, Vol. 21 ›› Issue (2): 263.

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Studies on the Preparation of Cr Nanometer Powder

CHENG Qi-Lin1, ZHAO Bin2, GU Hong-Chen1   

  1. 1. Institute of Technical Chemistry and Physics;
    2. Department of Chemistry, East China University of Science and Technology, Shanghai 200237, China
  • Received:1999-04-06 Online:2000-02-24 Published:2000-02-24

Abstract: Cr nanometer powder with mean diameter 50 nm was prepared in an organic solution of CrCl3, using sodium triethylborohydride as a reducing agent, toluene as a solvent, PVPas a dispersant, PdCl2as a nucleator. The temperature, the concentration of reactants and the addition of dispersant and nucleator were the main factors affecting the particle size. Also the mechanism and thermal stability of Cr nanometer powder were discussed.

Key words: Preparation of Cr nanometer powder, Dispersant, Nucleator, Thermal stability

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