A Study on Determination of Sulfide and Sulfite By Microwave Induced Plasma Atomic Emission Spectrometry with Gas Generation for Sample Introduction

Chem. J. Chinese Universities ›› 1992, Vol. 13 ›› Issue (11): 1364.

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A Study on Determination of Sulfide and Sulfite By Microwave Induced Plasma Atomic Emission Spectrometry with Gas Generation for Sample Introduction

ZHANG Jin-Sheng¹, ZHANG Han-Qi¹, DUAN Yi-Xiang¹, XU Fang¹, JIN Qin-Han¹, WANG Da-Ning², ZOU Ming-Qiang², LIU Li²

1. Department of Chemistry, Jilin University, Changchun, 130023;
2. Jilin Import and Export Commodity Inspection Bureau, Changchun

Received:1991-09-03 Revised:1992-05-01 Online:1992-11-24 Published:1992-11-24

Abstract

Abstract: In this paper,the determination of S^2- and SO₃^2- in solution were investigated by gas generation MIPAES.In the reaction cell S^2- and SO₃^2- reacted chemically with H₂SO₄ and formed H₂S and SO₂,respectively.The H₂S and SO₂ generated were carried into the MIP and the emission intensity at 216.9 nm was recorded.Various experimental conditions for determining S^2- and SO₃^2- were studied.The detection limits for S^2- and SO₃^2- are 0.08μg and 0.25μg.respectively.Good precision(RSD<5%)were observed either for S^2- or for SO₃^2-.

Key words: Microwave induced plasma atomic emission spectrometry, Sulfide, Sulfite

TrendMD:

ZHANG Jin-Sheng, ZHANG Han-Qi, DUAN Yi-Xiang, XU Fang, JIN Qin-Han, WANG Da-Ning, ZOU Ming-Qiang, LIU Li. A Study on Determination of Sulfide and Sulfite By Microwave Induced Plasma Atomic Emission Spectrometry with Gas Generation for Sample Introduction[J]. Chem. J. Chinese Universities, 1992, 13(11): 1364.

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A Study on Determination of Sulfide and Sulfite By Microwave Induced Plasma Atomic Emission Spectrometry with Gas Generation for Sample Introduction

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