Study on Gadolinium Nicotinate Coordination Compound with 1, 10-Phenanthroline

Abstract

Abstract: In this work, gadolinium nicotinate coordination compound with 1, 10-phenanthroline was synthesized and characterized as Gd(Phen)₂L₃ ·3H₂O(where HL = nicotinic acid, Phen = 1,10-phenanthroline) by chemical analysis, IRspectrum, thermal analysis, crystal structure analysis. The crystal is triclinic with coordination number eight. The parameters of unit cell are a= 9. 031Å , 6= 12. 857Å, c=17. 747Å.a=84. 923°, β=80. 564°, γ=84. 706°. The bccteriostatic tests show that Gd(Phen)₂L₃· 3H₂Ohas a stronger bacteriostasis than Phen and GdL₃· 2H₂O, especially to Candida albicans, hay bacillus and Pseudomonas aeruginosa.

Key words: 1, 10-Phenanthroline, Nicotlnic acid, Gadolinium, Structure, Bacteriostasis

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Zhang Zhongsheng, Wu Jigui, Deng Ruwen . Study on Gadolinium Nicotinate Coordination Compound with 1, 10-Phenanthroline[J]. Chem. J. Chinese Universities, 1990, 11(1): 7.

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Study on Gadolinium Nicotinate Coordination Compound with 1, 10-Phenanthroline

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