Chem. J. Chinese Universities ›› 2015, Vol. 36 ›› Issue (12): 2364.doi: 10.7503/cjcu20150464
• Articles: Inorganic Chemistry • Previous Articles Next Articles
SHI Xuanxuan, XIAO Ruijuan, WANG Zhen, ZHOU Jianping*(), BIAN Xiaobing
Received:
2015-06-12
Online:
2015-12-10
Published:
2015-11-17
Contact:
ZHOU Jianping
E-mail:zhoujp@snnu.edu.cn
Supported by:
CLC Number:
TrendMD:
SHI Xuanxuan, XIAO Ruijuan, WANG Zhen, ZHOU Jianping, BIAN Xiaobing. Effects of Magnetic Field on the Morphology and Properties of BiFeO3 Synthesized by Hydrothermal Method†[J]. Chem. J. Chinese Universities, 2015, 36(12): 2364.
Fig.1 XRD patterns of samples synthesized at 200 ℃ for 3 h with different KOH concentrations under magnetic fields of 0(A), 120 mT(B) and 240 mT(C) c(KOH)/(mol·L-1): a. 2; b. 3; c. 4; d. 5; e. 6; f. 7.
Fig.2 SEM images of samples synthesized at 200 ℃ for 3 h with c(KOH) of 4(A1—A3), 5(B1—B3) and 6 mol/L(C1—C3) under magnetic fields of 0(A1, B1, C1), 120 mT(A2, B2, B2), 240 mT(A3, B3, C3)
Fig.3 XRD patterns of samples synthesized at 140—220 ℃ for 3 h with c(KOH) of 4 mol/L under magnetic fields of 0(A), 120 mT(B) and 240 mT(C) Temperature/℃: a. 140; b. 150; c. 180; d. 200; e. 220.
Fig.4 SEM images of samples synthesized at temperature of 150 ℃(A1—A3), 180 ℃(B1—B3) and 200 ℃(C1—C3) for 3 h with c(KOH) of 4 mol/L under 0(A1, B1, C1), 120 mT(A2, B2, C2) and 240 mT(A3, B3, C3)
Fig.5 XRD patterns of samples synthesized at 200 ℃ with c(KOH) of 5 mol/L for different reaction time under magnetic fields of 0(A), 120 mT(B) and 240 mT(C) Reaction time/h: a. 1; b. 2; c. 3; d. 6; e. 9; f. 12.
Fig.6 SEM images of samples synthesized at 200 ℃ for 2 h(A1—A3), 6 h(B1—B3) and 9 h(C1—C3) with c(KOH) of 5 mol/L under magnetic fields of 0(A1, B1, C1), 120 mT(A2, B2, C2) and 240 mT(A3, B3, C3)
Fig.7 Photocatalytic degradation of MB over BiFeO3 powders synthesized at 200 ℃ for 3 h with c(KOH) of 4 mol/L(A) and 5 mol/L(B) under different magnetic fields
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