高等学校化学学报

高等学校化学学报 ›› 2002, Vol. 23 ›› Issue (7): 1241.

• 研究快报 • 上一篇    下一篇

具有内孔道的层状超分子化合物[(CuI)2(o-phen)2]的水热合成与晶体结构

王树涛1, 王恩波1, 李阳光1, 王力1, 胡长文1, 胡宁海2, 贾恒庆2   

  1. 1. 东北师范大学化学学院, 长春 130024;
    2. 中国科学院长春应用化学研究所, 长春 130022
  • 收稿日期:2002-01-25 出版日期:2002-07-24 发布日期:2002-07-24
  • 通讯作者: 王恩波(1936年出生),男,教授,博士生导师,主要从事多金属氧酸盐材料研究.
  • 基金资助:

    国家自然科学基金(批准号:201781010)

Hydrothermal Synthesis and Crystal Structure of a Layered Inner-tunnel Compound [(CuI)2(o-phen)2]

WANG Shu-Tao1, WANG En-Bo1, LI Yang-Guang1, WANG Li-HU Chang-Wen1, HU Ning-Hai1, JIA Heng-Qing2   

  1. 1. Faculty of Chemistry, Northeast Normal University, Changchun 130024, China;
    2. Changchun Institute of Applied Chemistry, Academia Sinica, Chang chun 130022, China
  • Received:2002-01-25 Online:2002-07-24 Published:2002-07-24

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关键词: 超分子, 氢键, 水热合成, 晶体结构

Abstract: Alayered inner tunnel supramolecular compound 1, [(CuI)2(o-phen)2], was hydrothermally synthesized and structurally characterized by X-ray crystal diffraction. It crystallizes in triclinic system, space group P1 with a=0.7759(2) nm, b=0.9070(2) nm, c=0.91894(10) nm, α=96306(14)°, β = 104.567(16)°, γ=109.421(19)°, V=0.5768(2)nm3, Z=1, R=0.0348, wR=0.0920.

Key words: Supramolecule, Hydrogen bonding, Hydrothermal synthesis, Crystal structure

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