Studies on Solid State Photochemical Syntheses and Inclusion Ability of New Host Compounds of Indoles

Chem. J. Chinese Universities ›› 1994, Vol. 15 ›› Issue (4): 528.

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Studies on Solid State Photochemical Syntheses and Inclusion Ability of New Host Compounds of Indoles

MENG Ji-Ben, DU Da-Ming, WANG Wen-Guang, WANG Yong-Mei

Department of Chemistry, Nankai University, Tianjin, 300071

Received:1993-04-29 Revised:1994-01-07 Online:1994-04-24 Published:1994-04-24

Abstract

Abstract: The photoreaction of terephthalicaldehyde, methyl p-formylbenzoate, and o-nitrobenzaldehyde with indole in the solid state gave five new products.Four of these products have a good inclusion ability.Products 1,2, 3 and 4 can form 1 : 1,1:2 or.2:1 inclusion complexes 1_a, 2_a, 3_a, 4_a and 4_b with acetone, ethyl acetate, carbon tetrachloride, and chloroform respectively.The structures of products or inclusion complexes were identified by IR,¹H NMR, MS and elemental analysis.X-ray diffraction analyses of inclusion complexes 1_a,2_a and 3_a were carried out to obtain more information about the structures.

Key words: Solid state photochemistry, Inclusion ability, Inclusion complex, Indole

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MENG Ji-Ben, DU Da-Ming, WANG Wen-Guang, WANG Yong-Mei. Studies on Solid State Photochemical Syntheses and Inclusion Ability of New Host Compounds of Indoles[J]. Chem. J. Chinese Universities, 1994, 15(4): 528.

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Studies on Solid State Photochemical Syntheses and Inclusion Ability of New Host Compounds of Indoles

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