Separation and Structural Identification of Hericium Erinaceur Oligosaccharide

Chem. J. Chinese Universities

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Separation and Structural Identification of Hericium Erinaceur Oligosaccharide

JIANG Rui-Zhi¹, WANG Ying², CHEN Ying-Hong¹, GAO Yang¹, HUANG En-Xi¹, GAO Qi-Pin³*

1. Academy of Chinese Medicine and Material Medical of Jilin Province, Changchun 130021, China;
2. School of Life Science, Jilin University, Changchun 130023, China;
3. Chinese Medicine and Material Medical University of Changchun, Centre of Study and Development, Changchun 130062, China

Received:2006-09-11 Revised:1900-01-01 Online:2007-07-10 Published:2007-07-10
Contact: GAO Qi-Pin

Abstract

Abstract:

It has been reported that the polysaccharide is the main active constituent of Hericium erinaceur. A series of oligosaccharide(mixtures of disaccharide and heptasaccharide of Hericium erinaceur) were separated from Hericium erinaceur by empty-fibrin filtration. Disaccharide and trisaccharide were purified via HPLC with NH₂ column. Component sugars and glycosidic linkage ways were analysed via GC and GC-MS. Electrospray ionization tandem mass spectrometry(MSⁿ) was used for the oligosaccharides structure study and the result shows that the disaccharide has two kind of structural styles and trisaccharide has one kind of structural style.

Key words: Hericium erinaceur, Oligosaccharide, Electrospray ionization tandem mass spectrometry

CLC Number:

O629
O657

TrendMD:

JIANG Rui-Zhi¹, WANG Ying², CHEN Ying-Hong¹, GAO Yang¹, HUANG En-Xi¹, GAO Qi-Pin³*. Separation and Structural Identification of Hericium Erinaceur Oligosaccharide[J]. Chem. J. Chinese Universities, doi: .

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Separation and Structural Identification of Hericium Erinaceur Oligosaccharide

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