Studies on the Wittig Reaction (XXIII)──Synthesis and Fungicidal Activities of 1-(1H-1,2, 4-Triazole-1-yl)-6-aryl-5-hexenyl aryl(alkyl) Ketones

Chem. J. Chinese Universities ›› 1995, Vol. 16 ›› Issue (9): 1396.

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Studies on the Wittig Reaction (XXIII)──Synthesis and Fungicidal Activities of 1-(1H-1,2, 4-Triazole-1-yl)-6-aryl-5-hexenyl aryl(alkyl) Ketones

DING Ming-Wu¹, SHI De-Qing¹, XIAO Wen-Jing¹, HUANG Wen-Fang¹, WU Tian-Jie²

1. Institute of Organic Synthesis, Wuhan, 430070;
2. Center of Analysis and Testing, Central China Normal University, Wuhan, 430070

Received:1994-09-19 Revised:1995-03-28 Online:1995-09-24 Published:1995-09-24

Abstract

Abstract: ω-Unsaturated bromides (2)were obtained from a solid/liquid transferred Wittig reaction of ω-bromobutyltriphenyl phosphonium bromide(1) with various substituted aromatic aldehydes.Then nine new title compounds(5) were synthesized from a solid/liquid transferred C-alkylation of 4 with 2.The fungicidal activities of some of the title compounds were studied.Some of them displayed potential fungicidal activities.

Key words: Wittig reaction, Synthesis, Phase transfer catalysis, Fungicide

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DING Ming-Wu, SHI De-Qing, XIAO Wen-Jing, HUANG Wen-Fang, WU Tian-Jie. Studies on the Wittig Reaction (XXIII)──Synthesis and Fungicidal Activities of 1-(1H-1,2, 4-Triazole-1-yl)-6-aryl-5-hexenyl aryl(alkyl) Ketones[J]. Chem. J. Chinese Universities, 1995, 16(9): 1396.

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Studies on the Wittig Reaction (XXIII)──Synthesis and Fungicidal Activities of 1-(1H-1,2, 4-Triazole-1-yl)-6-aryl-5-hexenyl aryl(alkyl) Ketones

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