Studies on the Determination of Trace Nitrite with K4Fe(CN)6-NO2-Luminol Chemiluminescence System

Chem. J. Chinese Universities ›› 1994, Vol. 15 ›› Issue (11): 1626.

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Studies on the Determination of Trace Nitrite with K₄Fe(CN)₆-NO₂-Luminol Chemiluminescence System

TANG Hong-Wu, LUO Qing-Yao, YU Xi-Mao, HE Zhi-Ke, ZENG Yun-E

Department of Chemistry, Wuhan University, Wuhan, 430072

Received:1993-12-20 Revised:1994-04-15 Online:1994-11-24 Published:1994-11-24

Abstract

Abstract: Anew chemiluminescence method for the determination of trace nitrite based on its oxidation of K₄Fe(CN)₆ is studied. The chemiluminescence signal arises from the reaction of luminol-K₃Fe(CN)₆.The detection limit is 3.6×10^-9g/mLfor nitrite, the calibration curve is rectilinear from 1×10^-8 to 6×10^-6g/mLof nitrite, and the relative standard deviation is 3.2%, This method has been applied to the analysis of natural waters, saliva and foods with satisfactory results.

Key words: Luminol, Chemiluminescence, Nitrite

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TANG Hong-Wu, LUO Qing-Yao, YU Xi-Mao, HE Zhi-Ke, ZENG Yun-E. Studies on the Determination of Trace Nitrite with K₄Fe(CN)₆-NO₂-Luminol Chemiluminescence System[J]. Chem. J. Chinese Universities, 1994, 15(11): 1626.

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Studies on the Determination of Trace Nitrite with K₄Fe(CN)₆-NO₂-Luminol Chemiluminescence System

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