Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)2][NiQ3](ClO4)

Chem. J. Chinese Universities ›› 1990, Vol. 11 ›› Issue (12): 1313.

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Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)₂][NiQ₃](ClO₄)

Zhang Ming-jie, Huang Chun-hui, Xu Guang-xian

Chemistry Department, Peking University, Beijing, 100871

Received:1990-07-17 Online:1990-12-24 Published:1990-12-24

Abstract

Abstract: Yttrium 8-quinolinol and nickel 8-quinolinol ionic adduct[YQ(HQ)₂][NiQ₃](ClO₄) was synthesized. The X-ray diffraction cryxtal structure of it showed that the crystal is monoclinic, space group P21/c with a=16.972(4)Å, b=14.128(3)Å, c = 22.615(4)Å,β=103. 16(2)°, V = 5280.14 Å³,F(000) = 2264, Z=4. [YQ(HQ)₂]²⁺ cation and [NiQ₃]^- anion were of six-coordinated octahedral geometry. Its IRspectra was recorded.

Key words: 8-Quinolinol, Yttrium, Nickel, Complex, Crystal structure

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Zhang Ming-jie, Huang Chun-hui, Xu Guang-xian . Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)₂][NiQ₃](ClO₄)[J]. Chem. J. Chinese Universities, 1990, 11(12): 1313.

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Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)₂][NiQ₃](ClO₄)

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