Chem. J. Chinese Universities ›› 2019, Vol. 40 ›› Issue (7): 1365.doi: 10.7503/cjcu20180831
• Article: Inorganic Chemistry • Previous Articles Next Articles
SHENG Bingchen1, LI Cong1, LIU Yingya1, WANG Anjie1, WANG Yao1,*(), ZHANG Jian2, LIU Weixu1
Received:
2018-12-12
Online:
2019-07-10
Published:
2019-07-12
Contact:
WANG Yao
E-mail:wangyao@dlut.edu.cn
Supported by:
CLC Number:
TrendMD:
SHENG Bingchen, LI Cong, LIU Yingya, WANG Anjie, WANG Yao, ZHANG Jian, LIU Weixu. Microfluidic Synthesis of UiO-66 Metal-organic Frameworks Modified with Different Functional Groups†[J]. Chem. J. Chinese Universities, 2019, 40(7): 1365.
Fig.2 XRD patterns of UiO-66 synthesized under different temperaturesFlowrate: 0.9 mL/min; residence time: 20 min. a. Simulated XRD pattern from single crystal X-ray diffraction; b. 120 ℃; c. 130 ℃; d. 140 ℃.
Fig.4 XRD patterns of UiO-66 synthesized under different flowrateResidence time: 20 min; reaction temperature: 130 ℃. Flowrate/(mL·min-1): a. 0.3; b. 0.6; c. 0.9; d. 1.2.
Fig.5 SEM images of UiO-66 synthesized under different flowrateResidence time: 20 min; reaction temperature: 130 ℃. Flowrate/(mL·min-1): (A) 0.6; (B) 0.9; (C) 1.2.
Fig.6 XRD patterns of UiO-66 synthesized under different residence timeFlowrate: 0.6 mL/min; reaction temperature: 130 ℃. Residence time/min: a. 10; b. 20; c. 40.
Fig.9 N2 adsorption-desorption isotherm of UiO-66 synthesized by microfluidic method(A) and the corresponding pore-size distribution plots and cumulative pore size distribution(B)
Fig.13 N2 adsorption-desorption isotherms(A1—A3), pore-size distribution plots and cumulative pore size distributions(B1—B3) of UiO-66-X synthesized by microfluidic method(A1, B1) UiO-66-NH2; (A2, B2) UiO-66-NO2; (A3, B3) UiO-66-Br.
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