Synthesis of a New Perylene Bisimide Dye Containing Melamine Moieties and Construction of Well-defined Nano-fiber

doi:10.7503/cjcu20121005

Chem. J. Chinese Universities ›› 2013, Vol. 34 ›› Issue (5): 1277.doi: 10.7503/cjcu20121005

• Polymer Chemistry • Previous Articles Next Articles

Synthesis of a New Perylene Bisimide Dye Containing Melamine Moieties and Construction of Well-defined Nano-fiber

DING Li-Wei¹, YANG Xin-Guo^1,2, ZHONG Wen-Bin¹, LIU Cun¹, LIU Zhen-Hui¹, ZHANG Feng-Ju¹

1. College of Materials Science & Engineering, Hunan University, Changsha 410082, China;
2. State Key Laboratory of Silicon Materials, Zhejiang University, Hangzhou 310027, China

Received:2012-11-05 Online:2013-05-10 Published:2013-05-10

Abstract

Abstract:

A new perylene diimide dye N,N'-bis[1,3,5-triazine-2,4-bis(dodecylamino)-6-amino]hexyl-3,4,9,10-perylene tetracarboxylic diimide(T-PTCD) was synthesized and characterized. Effect of polarity and volume ratio of solvents on the morphology of aggregates prepared by phase-transfer self-assembly or rapid solvent dispersion were comparatively investigated. Well-defined nano-fiber of T-PTCD was simply fabricated by the phase-transfer crystallization between methanol(as "bad" solvent) and chloroform(as "good" solvent). Low volume ratio of methanol and chloroform facilitates the formation of nano-fiber. When the volume ratio of methanol and chloroform is 1:4, the average diameter of T-PTCD nano-fiber is ca. 100 nm and the length is about 10 μm. In addition, the morphology of aggregates prepared by rapid solvent dispersion is significantly inferior to that by phase-transfer self-assembly.

Key words: Perylene bisimide, Nanofiber, Melamine, Phase-transfer self-assembly

CLC Number:

O625.8

TrendMD:

DING Li-Wei, YANG Xin-Guo, ZHONG Wen-Bin, LIU Cun, LIU Zhen-Hui, ZHANG Feng-Ju. Synthesis of a New Perylene Bisimide Dye Containing Melamine Moieties and Construction of Well-defined Nano-fiber[J]. Chem. J. Chinese Universities, 2013, 34(5): 1277.

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Synthesis of a New Perylene Bisimide Dye Containing Melamine Moieties and Construction of Well-defined Nano-fiber

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