高等学校化学学报

高等学校化学学报 ›› 2002, Vol. 23 ›› Issue (7): 1401.

• 研究简报 • 上一篇    下一篇

纳米Hg2Cl2/Al2O3有序阵列体系的制备和表征

王银海1, 牟季美2, 蔡维理2, 姚连增2, 刘艳美1   

  1. 1. 安徽大学物理系, 合肥 230039;
    2. 中国科学技术大学材料科学与工程系, 合肥 230026
  • 收稿日期:2000-08-23 出版日期:2002-07-24 发布日期:2002-07-24
  • 通讯作者: 王银海(1964年出生),男,博士,讲师,从事纳米结构材料研究.
  • 基金资助:

    国家自然科学基金(批准号:19974041);安徽省教育厅自然科学基金资助

Synthesis and Characterization of Nano-Hg2Cl2/Al2O3 Ordered Array System

WANG Yin-Hai1, MO Ji-Mei2, CAI Wei-Li2, YAO Lian-Zeng2, LIU Yan-Mei1   

  1. 1. Department of Physics of Anhui University, Hefei 230039, China;
    2. Department of Materials Science and Engineering of University, Science and Technology of China, Hefei 230026, China
  • Received:2000-08-23 Online:2002-07-24 Published:2002-07-24

PDF (PC)

关键词: 模板合成, 甘汞, 有序阵列, 电沉积

Abstract: We have prepared ordered porous alumina membrane. Metal Zn was deposited within the pores of alumina membrane by direct current. The alumina membrane with Zn in the pores was immersed in HgCl2 solution and Hg2Cl2/Al2O3 ordered array was synthesized by utilizing Zn reduced HgCl2. The XRDand TEMmeasuring demonstrated Hg2Cl2 located in the pores of alumina membrane and the diameters range from 30 to 80 nm.

Key words: Template synthesis, Calomel, Ordered array, Electrodeposition

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