Chem. J. Chinese Universities ›› 2022, Vol. 43 ›› Issue (9): 20220321.doi: 10.7503/cjcu20220321
• Perspectives • Previous Articles Next Articles
LIN Gaoxin1,2, WANG Jiacheng1,2()
Received:
2022-05-10
Online:
2022-09-10
Published:
2022-08-05
Contact:
WANG Jiacheng
E-mail:jiacheng.wang@mail.sic.ac.cn
Supported by:
CLC Number:
TrendMD:
LIN Gaoxin, WANG Jiacheng. Progress and Perspective on Molybdenum Disulfide with Single-atom Doping Toward Hydrogen Evolution[J]. Chem. J. Chinese Universities, 2022, 43(9): 20220321.
Fig.2 Active sites(edges, 1T phase, S vacancies and strain) of MoS2 for HER(A) and schematic illustration of Mo?SA?MoS2 in which Mo SAs are active sites for HER(B)[32]
Fig.3 Schematic procedure for syntheszing Cu@MoS2(A)[49] and schematic illustration of the preparation of Ni?SA?MoS2(B)[52](A) Copyright 2019, Elsevier B. V.; (B) Copyright 2018, Elsevier Ltd.
Catalyst | Synthesis method | Overpotential(at 10 mA/cm2)/mV | Electrolyte | Ref. |
---|---|---|---|---|
Co?MoS2 | Hydrothermal synthesis | 47 | 0.5 mol/L H2SO4 | [ |
Pt?MoS2 | Hydrothermal synthesis | 180 | 0.5 mol/L H2SO4 | [ |
Ru?MoS2 | Hydrothermal synthesis | 41 | 1 mol/L KOH | [ |
N?MoS2 | Hydrothermal synthesis | 168 | 0.5 mol/L H2SO4 | [ |
Ni?MoS2 | Hydrothermal synthesis | 127 | 0.5 mol/L H2SO4 | [ |
Ru, Ni?MoS2 | Wet?chemistry method | 31 | 1 mol/L KOH | [ |
Ru?MoS2 | Wet?chemistry method | 51 | 1 mol/L KOH | [ |
Ru?MoS2 | Wet?chemistry method | 30 | 1 mol/L KOH | [ |
Ru?MoS2 | Wet?chemistry method | 76 | 1 mol/L KOH | [ |
Co?MoS2 | Chemical vapor deposition | 137 | 0.5 mol/L H2SO4 | [ |
Ru?MoS2/MoP | Galvanostatic deposition | 45 | 1 mol/L KOH | [ |
Pt?MoS2 | Potential?cycling method | 88.4 | 1 mol/L KOH | [ |
Pt?MoS2 | Solar irradiation | 44 | 0.5 mol/L H2SO4 | [ |
U?MoS2 | Pulse voltammetry method | 72 | 1 mol/L KOH | [ |
Table 1 Electrocatalytic HER performance of different SAs doped MoS2
Catalyst | Synthesis method | Overpotential(at 10 mA/cm2)/mV | Electrolyte | Ref. |
---|---|---|---|---|
Co?MoS2 | Hydrothermal synthesis | 47 | 0.5 mol/L H2SO4 | [ |
Pt?MoS2 | Hydrothermal synthesis | 180 | 0.5 mol/L H2SO4 | [ |
Ru?MoS2 | Hydrothermal synthesis | 41 | 1 mol/L KOH | [ |
N?MoS2 | Hydrothermal synthesis | 168 | 0.5 mol/L H2SO4 | [ |
Ni?MoS2 | Hydrothermal synthesis | 127 | 0.5 mol/L H2SO4 | [ |
Ru, Ni?MoS2 | Wet?chemistry method | 31 | 1 mol/L KOH | [ |
Ru?MoS2 | Wet?chemistry method | 51 | 1 mol/L KOH | [ |
Ru?MoS2 | Wet?chemistry method | 30 | 1 mol/L KOH | [ |
Ru?MoS2 | Wet?chemistry method | 76 | 1 mol/L KOH | [ |
Co?MoS2 | Chemical vapor deposition | 137 | 0.5 mol/L H2SO4 | [ |
Ru?MoS2/MoP | Galvanostatic deposition | 45 | 1 mol/L KOH | [ |
Pt?MoS2 | Potential?cycling method | 88.4 | 1 mol/L KOH | [ |
Pt?MoS2 | Solar irradiation | 44 | 0.5 mol/L H2SO4 | [ |
U?MoS2 | Pulse voltammetry method | 72 | 1 mol/L KOH | [ |
Fig.4 HAADF?STEM image(A) and corresponding enlarged image(B) of Ru/Ni?MoS2, HAADF intensity line profiles taken along the appropriately numbered lines indicated in (A) and (B)(C)[60], TEM image of Pt?MoS2 with the inset showing a typical MoS2 layer distance of 0.62 nm(D), HAADF?STEM images of Pt?MoS2 showing that the single Pt atoms marked by red circles uniformly disperse in the 2D MoS2 plane(E), enlarged image showing a honeycomb arrangement of MoS2(F), and the single Pt atoms occupying the exact positions of the Mo atoms(marked by red arrows)(G), the k2?weighted EXAFS spectra(H) and the normalized Pt L3?edge XANES spectra(I)[68](G) The bottom inset shows the simulated configuration of Pt-MoS2. The green, yellow and blue balls represent Mo, S and Pt, respectively. (A)—(C) Copyright 2021, Elsevier B. V.; (D)—(I) Copyright 2015, Royal Society of Chemistry.
Fig.5 FT?EXAFS spectra(A), schematic of the atomic structure of Ru/Lnp?MoS2 and Ru/np?MoS2 derived from(A)(B, C)[? in (C) represents the amount of deformation], polarization curves(D), corresponding Tafel plots derived from (D)(E), ECSA?normalized polarization curves(F), ECSA?normalized current density at an overpotential of 100 mV(G)(the average diameters of ligaments for Ru/LnpMoS2 and Ru/np?MoS2 were also shown), and stability measurement of Ru/np?MoS2 at an overpotential of 30 mV(H)[29]
Fig.6 Adsorption free energies of H*(ΔGH*) at different catalysts(A), adsorption models of H* at different sites of Co/Se?MoS2(B), relative formation energies of the Co/Se?co?doped MoS2 with different doping configurations of Co and Se being separated(Co/Se?separated, grid bars) or adjacent (Co/Se?adjacent, solid bars) to each other(C), structures of Co/Se?co?doped basal plane, Mo?edge, and S?edge with Co/Se?separated and Co/Se?adjacent configurations(D)[86]
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