Surface Desorption Atmospheric Pressure Chemical Ionization Mass Spectrometry for Direct Detection of Trace Amounts of Cocaine in Hot Pot Sauce Materials

Chem. J. Chinese Universities ›› 2010, Vol. 31 ›› Issue (10): 1961.

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Surface Desorption Atmospheric Pressure Chemical Ionization Mass Spectrometry for Direct Detection of Trace Amounts of Cocaine in Hot Pot Sauce Materials

SONG Qing-Hao1,3, WANG Jiang2, HU Bin2, CHEN Huan-Wen2, JIN Qin-Han1*

1. Research Center for Analytical Instrumentation, Institute of Cyber-Systems and Control, State Key Laboratory of Industrial Control Technology, Zhejiang University, Hangzhou 310058, China;
2. Department of Applied Chemistry, East China Institute of Technology, Fuzhou 344000, China;
3. Shandong Electric Power Engineering Consulting Institute, Jinan 250013, China

Received:2010-02-05 Online:2010-10-10 Published:2010-10-10
Contact: JIN Qin-Han. E-mail: qhjin@zju.edu.cn
Supported by:
东华理工大学研究生创新资金(批准号: DYCA10002)资助.

Abstract

Abstract: A novel method was developed for the direct detection of cocaine in hot pot sauce materials by surface desorption atmospheric pressure chemical ionization mass spectrometry(SDAPCI-MS) without any sample pretreatment. By using sample needle sampling, the volume of each sampling was at nanoliter level. The ave-rage time for a single sample analysis was less than 0.5 min. The recoveries of six samples spiked with cocaine were shown to be in the range of 92.9%—106.6%, and the relative standard deviations of the method were in the range of 5.2%—11.8%. The detection limit of this method for cocaine was found to be 1.5×10-12 g/mL. The data show SDAPCI-MSn is a powerful tool for rapid, semi-quantitative detection of cocaine in hot pot sauce materials.

Key words: Surface desorption atmospheric pressure chemical ionization, Mass spectrometry, Cocaine, Hot pot sauce materials, Rapid analysis

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SONG Qing-Hao, WANG Jiang, HU Bin, CHEN Huan-Wen, JIN Qin-Han*. Surface Desorption Atmospheric Pressure Chemical Ionization Mass Spectrometry for Direct Detection of Trace Amounts of Cocaine in Hot Pot Sauce Materials[J]. Chem. J. Chinese Universities, 2010, 31(10): 1961.

References

[1]Fernández P., Lafuente N., Cruz A., López-Rivadulla M., Cruz A.. J. Anal. Toxicol[J], 1996, 20(4): 224—228 [2]JIANG He-Ping(蒋和平). Journal of Sichuan University, Natural Science Edition(四川大学学报自然科学版)[J], 2005, 42(4): 794—797 [3]Saito T., Mase H., Takeichi S., Inokuchi S.. J. Pharm. Biomed. Anal.[J], 2007, 43(1): 358—363 [4]FANG Huai-Fang(方怀防), ZENG Zhao-Rui(曾昭睿), LIU Lan(刘岚), PANG Dai-Wen(庞代文). Chem. J. Chinese Universities(高等学校化学学报)[J], 2006, 27(5): 856—858 [5]Jagerdeo E., Abdel-rehim M.. J. Am. Soc. Mass Spectrom.[J], 2009, 20(5): 891—899 [6]Hu B., Peng X. J., Yang S. P., Gu H., Chen H. W., Huan Y. F., Zhang T. T., Qiao X. L.. J. Am. Soc. Mass Spectrom.[J], 2009, 21(2): 290—293 [7]DING Jian-Hua(丁健桦), YANG Shui-Ping(杨水平), LIU Qing(刘清), WU Zhuan-Zhang(吴转璋), CHEN Huan-Wen(陈焕文), REN Yu-Lin(任玉林), ZHENG Jian(郑健), LIU Qing-Jun(刘清珺). Chem. J. Chinese Universities(高等学校化学学报)[J], 2009, 30(8): 1533—1537 [8]CHEN Huan-Wen(陈焕文), LAI Jin-Hu(赖劲虎), ZHOU Yu-Fen(周瑜芬), LI Jian-Qiang(李健强), ZHANG Xie(张燮), LUO Ming-Biao(罗明标), WANG Zhi-Chang(王志畅). Chinese J. Anal. Chem.(分析化学) [J], 2007, 35(8): 1233—1235 [9]Chen H. W., Zheng J., Zhang X., Luo M. B., Wang Z. C., Qiao X. L.. J. Mass Spectrom.[J], 2007, 42(8): 1045—1056 [10]Chen H. W., Liang H. Z., Ding J.H., Qiao X. L.. Journal of Agricultural and Food Chemistry [J], 2007, 55: 10093—10100 [11]YANG Shui-Ping(杨水平), CHEN Huan-Wen(陈焕文), YANG Yu-Ling(杨宇玲), HU Bin(胡斌), ZHANG Xie(张燮), ZHOU Yu-Fen(周瑜芬), ZHANG Li-Li(张丽丽), GU Hai-Wei(顾海威). Chinese J. Anal. Chem.(分析化学) [J], 2009, 37(3): 315—318 [12]YANG Shui-Ping(杨水平), HU Bin(胡斌), LI Jian-Qiang(李建强), HAN Jing(韩京), ZHANG Xie(张燮), CHEN Huan-Wen(陈焕文), LIU Qing(刘清), LIU Qing-Jun(刘清珺), ZHENG Jian(郑健). Chinese J. Anal. Chem.(分析化学) [J], 2009, 37(5): 691—694 [13]LIANG Hua-Zheng(梁华正), CHEN Huan-Wen(陈焕文). Chinese J. Appl. Chem.(应用化学)[J], 2008, 25(5): 519—523 [14]Yang S. P., Ding J.H., Zheng J., Hu B., Li J. Q., Chen H. W., Zhou Z. Q., Qiao X. L.. Anal. Chem.[J], 2009, 81: 2426—2436 [15]WANG Jiang(王姜), YANG Shui-Ping(杨水平), YAN Fei-Yan(鄢飞燕), LIU Yan(刘艳), LI Ming(李明), SONG Yu-Hang(宋宇航), ZHAN Ye-Bing(占叶兵), CHEN Huan-Wen(陈焕文). Chinese J. Anal. Chem.(分析化学)[J], 2010, 38(4): 453—457 [16]Wang P. P., Bartlett M. G.. J. Mass Spectrom.[J], 1998, 33: 961—967

Surface Desorption Atmospheric Pressure Chemical Ionization Mass Spectrometry for Direct Detection of Trace Amounts of Cocaine in Hot Pot Sauce Materials

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