Preparation and Characterization of Nickel Hydroxide Nanorods Using Hydrothermal Synthesis Method

Abstract

Abstract: Nickel hydroxide nanorods were prepared by using hydrothermal synthesis method. The structures of Ni(OH)₂ were characterized by X-ray diffractometer. The morphologies were observed by using TEM. The influences of hydrothermal reaction temperature and pH values on the morphologies and structure of the products were investigated. It was found that the best conditions for preparing nickel hydroxide nanorods were the reaction temperature in the range 180～200 ℃ and the pH value between 9 and 10.

Key words: Nickel hydroxide, Nanorods, Hydrothermal synthesis

CLC Number:

O614.4

TrendMD:

TIAN Zhou-Ling, JIAO Qing-Ze, ZHAO Yun . Preparation and Characterization of Nickel Hydroxide Nanorods Using Hydrothermal Synthesis Method[J]. Chem. J. Chinese Universities, 2005, 26(8): 1387.

References

[1] Zhou S.X.,Li J.M.,Ke Y.X.et al..Mater.Lett.[J],2003,57:2602_2605 [2] Cao M.H.,Hu C.W.,Wang Y.H.et al..Chem.Comm un.[J],2003:1884_1885 [3] GU O Min(郭敏),D IAO Peng(刁鹏),CA I Sheng-Min(蔡生民).Chem.J.Ch inese Un iversities(高等学校化学学报)[J],2004,25(2):345_347 [4] Hu J.Q.,Deng B.,Zhang W.X.et al..In ter.J.Ino rg.Mater.[J],2001,3:639_642 [5] Nie Q.L.,Xu Z.D.,Yuan Q.L.et al..Mater.Chem.Phys.[J],2003,82:808—811 [6] GU O Bing-Kun(郭炳),L I Xin-Hai(李新海),YAN G Song-Qing(杨松青).Chem istry Electrical Sou rce——Battery Princip le and Prep aration Techno logy(化学电源——电池原理及制备技术)[M],Chang sha:Cen tral Sou th Un iversity Press,2003:208_209 [7] Cai F.S.,Zhang G.Y.,Chen J.et al..Angw.Chem.In t.Ed s.[J],2003,43(32):4212_4216 [8] ZHAO Li(赵力),ZHOU De-Ru i(周德瑞),ZHAN G Cu i-Fen(张翠芬).Chem.On line(化学通报)[J],2001,(8):513_515 [9] HAN Xi-Jiang(韩喜江),X IE Xiao-Mei(谢小美),XU Chong-Quan(徐崇泉)et al..Ch in.J.Ino rg.Chem.(无机化学学报)[J],2003,19(3):247_251 [10] Zhang Y.S.,Zhou Z.,Yan J..J.Pow er Sou r.[J],1998,75:283_287 [11] Liang Z.H.,Zhu Y.J.,Hu X.L..J.Phys.Chem.B[J],2004,108:3488_3491 [12] Li X.L.,Liu J.F.,Li Y.D..Mater.Chem.Phys.[J],2003,80:223_227 [13] Liang J.H.,Li Y.D..Chem.Lett.[J],2003,32(12):1126_1127 [14] L I Shu-Tang(李树棠).Elem en ts of X-ray Diffraction fo r Crystal(晶体X射线衍射学基础)[M],Chang sha:Met allu rgy Press, 1990:106_109 [15] XU Ru-Ren(徐如人),PAN G Wen-Qin(庞文琴).Ino rgan ic Syn thesis and Prep arative Chem istry(无机合成与制备化学)[M], Beijing:Higher Education Press,1991:133_134 [16] Wang X.,Li Y.D..Angew.Chem.In t.Ed.[J],2002,41(24):4790_4793 [17] Wang X.,Li Y.D..Chem.Eu r.J.[J],2003,9(1):300_306 [18] Peng Z.A.,Peng X.G..J.Am.Chem.Soc.[J],2001,123:1389_1395 [19] Peng Z.A.,Peng X.G..J.Am.Chem.Soc.[J],2002,124:3343_3353