Chem. J. Chinese Universities ›› 1995, Vol. 16 ›› Issue (6): 836.

• Articles • Previous Articles     Next Articles

Hydrothermal Synthesis and Characterization of a New Layered Potassium Phosphatoantimonate

AN Yong-Lin1, FENG Shou-Hua1, LI Lian-Sheng1, XU Ru-Ren1, YUE Yong2   

  1. 1. Key Laboratory of Inorganic Hydrothermal Synthesis, Jilin University, Changchun 130023;
    2. Wuhan Institute of Physics Chinese Academy of Sciences
  • Received:1994-08-23 Revised:1994-12-20 Online:1995-06-24 Published:1995-06-24

Abstract: Anew potassium phosphatoantimonate with composition of 4K2O·4Sb2O5·P2O5·8H2O was synthesized by hydrothermal method,and characterized by SEM,XRD,XPS, 31PMAS NMR,IR techniques.This compound has a layered structure,into which the amine can be intercalated,and the Kions can be exchanged.

Key words: Phosphatoantimonate, Hydrothermal synthesis, Characterization

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