The Application of Micellar Electrokinetic Capillary Chromatography to Analysis in the Synthesis of Mandelic Acid

Chem. J. Chinese Universities ›› 1992, Vol. 13 ›› Issue (1): 45.

• Articles • Previous Articles Next Articles

The Application of Micellar Electrokinetic Capillary Chromatography to Analysis in the Synthesis of Mandelic Acid

FU Xiao-yun¹, LU Jian-de¹, LU Yi-jing², XU Hui-feng²

1. The Center of Analysis and Testing, Zhe Jiang University, Hangzhou, 310027;
2. Department of Chemistry, Zhe Jiang University

Received:1990-12-04 Online:1992-01-24 Published:1992-01-24

Abstract

Abstract: The fast and simultaneous analysis of benzyl alcohol, benzaldehyde, benzoic acid and mandelic acid was studied by Micellar Electrokinetic Capillary Chromatography (MECC).The raw material, semifinished products and purified products in the synthesis of mandelic acid were analyzed.The samples synthesized under different conditions were analyzed by using internal standard method.The resutls were used to optimize the synthesis of mandelic acid.

Key words: Micellar Electrokinetic Capillary Chromatograph, Mandelic acid, Benzaldehyde, Benzole acid

TrendMD:

FU Xiao-yun, LU Jian-de, LU Yi-jing, XU Hui-feng. The Application of Micellar Electrokinetic Capillary Chromatography to Analysis in the Synthesis of Mandelic Acid[J]. Chem. J. Chinese Universities, 1992, 13(1): 45.

[1]	HUANG Rui,YAO Zhilong,SUN Peiyong,ZHANG Shenghong. Effect of Structure and Properties of CuO-WO₃-ZrO₂ on Hydrogenation Catalytic of Benzaldehyde^† [J]. Chem. J. Chinese Universities, 2019, 40(5): 1005.
[2]	DONG Gaoyun,LI Rui,FAN Tingting,LI Jiajia,LI Xia. Luminescence Sensing of Benzaldehyde and Cation of 3-(2-Carboxy-phenoxy)-phthalicate-based Lanthanide Complexes^† [J]. Chem. J. Chinese Universities, 2016, 37(8): 1421.
[3]	HUANG Xiao, GAN Hanlin, PENG Liang, GU Fenglong. Theoretical Study on the Selective Redox Mechanism of Benzaldehyde in Photo-catalyzed Reaction^† [J]. Chem. J. Chinese Universities, 2016, 37(2): 297.
[4]	LI Ming, LI Youji, XU Peng, LIN Xiao, HAN Wenxuan. Preparation and Photoelectrocatalytic Performance of Mesoporous Titanium Dioxide/Conductive Carbon Felt Electrode^† [J]. Chem. J. Chinese Universities, 2015, 36(8): 1596.
[5]	WANG Kai, WANG Qinglei, YAN Tingting, LIN Aolei. Raman Spectroscopic Study on High Pressure-induced Phase Transition of D,L-Mandelic^† [J]. Chem. J. Chinese Universities, 2015, 36(2): 381.
[6]	ZHANG Hui, HE Yuhan, TANG Duo, LI Yanwei. In-cell Selective Ultrasonic Electrosynthesis of Methyl Benzaldehyde Based on RBF Neural Network and Genetic Algorithm^† [J]. Chem. J. Chinese Universities, 2014, 35(6): 1199.
[7]	LV Ze-Liang, GAO Yang, LI Jun, HUANG Tong-Kun, HE Shu-Jie, ZOU Yong. Synthesis and Antitumor Activities of 3-Arylbenzofunanone Analogues [J]. Chem. J. Chinese Universities, 2013, 34(11): 2531.
[8]	HAN Bing-Xing, WU Fang-Ying. Synthesis of N,N-Dimethyl Pyridine Benzaldehyde-4-dimethylaminobenzoylhydrazone and Its Application for Selective Recognizing Cu²⁺ [J]. Chem. J. Chinese Universities, 2013, 34(11): 2483.
[9]	XIAO Min, ZHANG Li-Na, WU Fang-Ying. Synthesis of 2'-Borono-benzaldehyde-7-(8-hydroxy-5-sulfoacid) Quinoline Hydrazone and Recognition of Pb²⁺ [J]. Chem. J. Chinese Universities, 2012, 33(05): 919.
[10]	LI Yan-Wei, JIANG Guang-Ce, ZHANG Chuan-Guang, WEI Wen-Long. Synthesis of Benzaldehyde and Succinic Acid by Paired Electrosynthesis with On-line Ultrasound [J]. Chem. J. Chinese Universities, 2012, 33(01): 66.
[11]	GUO Zhi-Feng, LI Fen-Fang*, XING Jian-Min. Chiral Recognition of α-Cyclohexyl-mandelic Acid in Alcohol/Salt-based Aqueous Two-phase Systems [J]. Chem. J. Chinese Universities, 2011, 32(2): 275.
[12]	WANG Zhan-Liang, ZHU Dong-Sheng, WANG Rong-Shun. Synthesis, Crystal Structure and Antibacterial Activity of Two Novel Complexes of N,N'*-Bis(o-oxy-acetate)benzylpropylenediamine with Cu(Ⅱ) and Ni(Ⅱ) and a Complex N-(o-oxy-acetate)benzylpropylenediamine with Cu(Ⅱ) [J]. Chem. J. Chinese Universities, 2008, 29(5): 876.
[13]	LI Hui¹, WANG Jing², QIN Feng-Mei¹, ZHOU Dao-Wei ^1* , ZHU Dong-Sheng ^2*. Synthesis, Crystal Structure and Bioactivity of two Novel Complexes N,N′-Bis(o-oxy-acetate)benzylethylenediamine with Co(Ⅱ) and N-(o-oxy-acetate)benzylethylene Diamine with Cu(Ⅱ) [J]. Chem. J. Chinese Universities, 2006, 27(5): 821.
[14]	MU Jin-Xia, YIN Xue-Feng, WANG Yan-Guang. Synthesis of 4-Methoxybenzaldehyde Oxime in a Microfluidic Chip [J]. Chem. J. Chinese Universities, 2006, 27(11): 2114.
[15]	ZHANG Lan, LI Rui-Bao, TONG Ping, CHEN Guo-Nan . Micellar Electrokinetic Capillary Chromatography Study of Adenine and Purine of Anti-cancer Medicine [J]. Chem. J. Chinese Universities, 2005, 26(8): 1437.

The Application of Micellar Electrokinetic Capillary Chromatography to Analysis in the Synthesis of Mandelic Acid

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments