Chem. J. Chinese Universities ›› 2017, Vol. 38 ›› Issue (12): 2169.doi: 10.7503/cjcu20170251
• Analytical Chemistry • Previous Articles Next Articles
YU Xijuan*(), HAN Lulu, HUN Xu
Received:
2017-05-09
Online:
2017-12-10
Published:
2017-11-07
Contact:
YU Xijuan
E-mail:xjuanyu@qust.edu.cn
Supported by:
TrendMD:
YU Xijuan, HAN Lulu, HUN Xu. Cu2+ Modified Gold Nanoclusters for Fluorescence Turn-on Detection of Dopamine†[J]. Chem. J. Chinese Universities, 2017, 38(12): 2169.
Fig.2 Fluorescence excitation(a) and emission(b) spectra of the AuNCs@11-MUA Inset shows photographs of the AuNCs@11-MUA under 365 nm UV light illumination(left) and sunlight(right).
Method | Liner range/(μmol·L-1) | LOD/(μmol·L-1) | Ref. |
---|---|---|---|
ECL | 0.1—50.0 | 0.040 | [ |
ECL | 0.2—70.0 | 0.067 | [ |
GC/MS | 1.41—2.74 | 0.004 | [ |
DPV | 0.05—10.0 | 0.033 | [ |
DPV | 0.2—30.0 | 0.080 | [ |
FL | 0.1—20.0 | 0.029 | [ |
FL | 0.05—8.0 | 0.018 | [ |
FL | 0.20—50.0 | 0.080 | This work |
Table 1 Analytical performance of this method compared with other methods
Method | Liner range/(μmol·L-1) | LOD/(μmol·L-1) | Ref. |
---|---|---|---|
ECL | 0.1—50.0 | 0.040 | [ |
ECL | 0.2—70.0 | 0.067 | [ |
GC/MS | 1.41—2.74 | 0.004 | [ |
DPV | 0.05—10.0 | 0.033 | [ |
DPV | 0.2—30.0 | 0.080 | [ |
FL | 0.1—20.0 | 0.029 | [ |
FL | 0.05—8.0 | 0.018 | [ |
FL | 0.20—50.0 | 0.080 | This work |
Fig.12 Selectivity of the assay for DAa. Ascorbic acid; b. uric acid; c. glycine; d. valine; e. methionine;f. tyrosine; g. tryptophan; h. L-lysine; i. L-cysteine; j. glutathione;k. Ca2+; l. K+; m. Na+; n. Cl-; o. NO3-; p. DA.
Sample | Spiked DA/(μmol·L-1) | Found/(μmol·L-1) | Recovery(%) | RSD(%) |
---|---|---|---|---|
Human serum 1 | 10.0 | 9.71 | 97.1 | 4.08 |
Human serum 2 | 20.0 | 18.64 | 93.2 | 1.75 |
Human serum 3 | 30.0 | 28.95 | 96.5 | 2.76 |
Human urine 1 | 10.0 | 9.73 | 97.3 | 2.6 |
Human urine 2 | 20.0 | 18.96 | 94.8 | 3.9 |
Human urine 3 | 30.0 | 28.68 | 95.6 | 2.7 |
Table 2 Determination of dopamine in serum or urine samples(n=5)
Sample | Spiked DA/(μmol·L-1) | Found/(μmol·L-1) | Recovery(%) | RSD(%) |
---|---|---|---|---|
Human serum 1 | 10.0 | 9.71 | 97.1 | 4.08 |
Human serum 2 | 20.0 | 18.64 | 93.2 | 1.75 |
Human serum 3 | 30.0 | 28.95 | 96.5 | 2.76 |
Human urine 1 | 10.0 | 9.73 | 97.3 | 2.6 |
Human urine 2 | 20.0 | 18.96 | 94.8 | 3.9 |
Human urine 3 | 30.0 | 28.68 | 95.6 | 2.7 |
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