高等学校化学学报 ›› 2003, Vol. 24 ›› Issue (12): 2155.

• 研究简报 • 上一篇    下一篇

三元金属二硫化物纳米管的制备

李国华, 徐铸德, 陈卫祥, 聂秋林, 夏军保   

  1. 浙江大学化学系, 杭州 310027
  • 收稿日期:2003-01-06 出版日期:2003-12-24 发布日期:2003-12-24
  • 通讯作者: 徐铸德(1944年出生),男,博士,教授,从事化学动力学和无机纳米材料研究.E-mail:xuzhude@css.zju.edu.cn E-mail:xuzhude@css.zju.edu.cn
  • 基金资助:

    国家自然科学基金(批准号:20171039,50171063)资助

Preparation of Ternary Metals Disulfide Nanotube

LI Guo-Hua, XU Zhu-De, CHEN Wei-Xiang, NIE Qiu-Lin, XIA Jun-Bao   

  1. Department of Chemistry, Zhejiang University, Hangzhou 310027, China
  • Received:2003-01-06 Online:2003-12-24 Published:2003-12-24

关键词: 剥离-重新堆垛-结构控制, 三元金属二硫化物, 纳米管, 制备

Abstract: Ternary metals disulfide nano-compound, Mnx(MoW)1-xS2, was prepared by exfoliating-restacking-structure controlling approach, and characterized by XRD, TEM, SAED and EDS respectively. XRDresults show that the phases of the intermediate were composed of MoS2, WS2, MnCl2·H2O and one unclear phase. The end product was composed of MnS2, MoS2and WS2phases. TEM results show that the morphologies of the sample are nano-tubular with ringent. EDS results show that the components of nanotube is Mnx(MoW)1-xS2.More detailed work is needed to study the precise structure and formation mechanism for sure.

Key words: Exfoliating-restacking-structure controlling, Ternary metals disulfide, Nanotube, Preparation

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