Synthesis and Crystal Structure of (±)-1-[(2-Hydroxy-5-methylphenyl) (phenyl)methyl]-2-pyridylbenzimidazole

Chem. J. Chinese Universities ›› 2000, Vol. 21 ›› Issue (12): 1861.

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Synthesis and Crystal Structure of (±)-1-[(2-Hydroxy-5-methylphenyl) (phenyl)methyl]-2-pyridylbenzimidazole

WANG Jin-Yi¹, ZHOU Jing¹, CHENG Dong-Liang¹, JIAN Pan-Ming²

1. Department of Chemistry, Lanzhou University, Lanzhou 730000, China;
2. Department of Chemistry, Yangzhou University, Yangzhou 225002, China;
3. Chengdu Instituteof Biology, Chinese Academy of Sciences, Chengdu 610041, China

Received:1999-11-22 Online:2000-12-24 Published:2000-12-24

Abstract

Abstract: (±)-1-[(2-Hydroxy-5-methylphenyl) (phenyl)methyl]-2-pyridylbenzimidazole was synthesized and its crystal structure was determined by Xray four cycle diffraction method.The crystal belongs to monoclinic, space group P2₁/c , with the crystal cell parameters: a =1.3514(5) nm, b =0.9659(6) nm, c =1.6740(3) nm, β =110.27(2)°, V =2.0497(14) nm³, Z=4, Dc=1.269 g/cm³, R₁= 0.0575 . The analyses of crystal structure show that the chain structure is formed by intermolecular Hbond

Key words: (±)-Benzimidazole, Synthesis, Crystal structure

CLC Number:

O626.23

TrendMD:

WANG Jin-Yi, ZHOU Jing, CHENG Dong-Liang, JIAN Pan-Ming. Synthesis and Crystal Structure of (±)-1-[(2-Hydroxy-5-methylphenyl) (phenyl)methyl]-2-pyridylbenzimidazole[J]. Chem. J. Chinese Universities, 2000, 21(12): 1861.

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Synthesis and Crystal Structure of (±)-1-[(2-Hydroxy-5-methylphenyl) (phenyl)methyl]-2-pyridylbenzimidazole

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