Synthesis of 1-Aryloxyacetyl-4-(2-nitrobenzoyl)-thiosemicarbazides and Related Heterocyclic Compounds

Abstract

Abstract: Ten new 1-aryloxyacetyl-4-(2-nitrobenzoyl)-thiosemicarbazides(Ⅲ) were synthesized under the condition of solid-liquid phase transfer catalysis, and compounds Ⅲ on fur-ther reaction with acetic acid gives ten 2-(2-nitrobenzoylamido)-5-aryloxymethyl-1,3,4-thia-diazoles(Ⅳ). Compounds Ⅲ and Ⅳ were characterized by elemental analysis, IR and ¹HNMR. The preliminary promoting effects of compounds Ⅲ and Ⅳ on wheat growth were also tested.

Key words: 1-Aryloxyacetyl-4-(2-nitrobenzoyl)-thiosemicarbazide, 1,3,4-Thiadiazole, Phase transfer catalysis, Synthesis

CLC Number:

O626

TrendMD:

WANG Xi-Cun, YU Tian-Zhi, LI Zheng, CHEN Ji-Chou, WANG Xiu-Chun  . Synthesis of 1-Aryloxyacetyl-4-(2-nitrobenzoyl)-thiosemicarbazides and Related Heterocyclic Compounds[J]. Chem. J. Chinese Universities, 1999, 20(10): 1581.

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Synthesis of 1-Aryloxyacetyl-4-(2-nitrobenzoyl)-thiosemicarbazides and Related Heterocyclic Compounds

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