Addition Recation of Buckminsterfullerent with Amines and Electrospray Ionization Mass Spectrometry Determination of Reaction Products

Chem. J. Chinese Universities ›› 1996, Vol. 17 ›› Issue (10): 1570.

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Addition Recation of Buckminsterfullerent with Amines and Electrospray Ionization Mass Spectrometry Determination of Reaction Products

WEI Xian-Wen¹, WU Ming-Fei¹, ZHANG Cheng¹, QI Ling¹, XU Zheng¹, CAO Ya-Cheng², ZHOU Ke-Yu²

1. Coordination Chemistry Institute, State Key Laboratory of Coordination Chemistry, Nanjing University, Nanjing, 210093;
2. Nanjing Institute of Soil, Chinese Academy of Sciences

Received:1995-11-28 Online:1996-10-24 Published:1996-10-24

Abstract

Abstract: The addition reactions of C₆₀ with trimethylenediamine and 3-dimethyl-aminopropylamine were reported.The reaction products were determined directly by ESI-MSwithout pre-ionization.The reaction product precipitated from toluene,which prevented from polyaminates and led the mono-diamine adduct as a main product.Addition to main product there are some C₆₀O_n(NH₂CH)₂CH₂CH₂NR₂)_m(R=H,CH₃) when the reaction runs at open air.The mono-diamine adduct may be gotten with control reaction condition.

Key words: C₆₀ chemistry, Aminates, ESI-MS

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WEI Xian-Wen, WU Ming-Fei, ZHANG Cheng, QI Ling, XU Zheng, CAO Ya-Cheng, ZHOU Ke-Yu. Addition Recation of Buckminsterfullerent with Amines and Electrospray Ionization Mass Spectrometry Determination of Reaction Products[J]. Chem. J. Chinese Universities, 1996, 17(10): 1570.

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Addition Recation of Buckminsterfullerent with Amines and Electrospray Ionization Mass Spectrometry Determination of Reaction Products

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