Chem. J. Chinese Universities ›› 1991, Vol. 12 ›› Issue (11): 1542.

• Articles • Previous Articles     Next Articles

Synthesis of Perovskite-type Nanocrystalline Material Complex Oxide LaFeO3by Citrate Process

Li Xi1, Zhao Mu-yu1, Wang Zi-chen1, Xu Bao-kun2   

  1. 1. Department of Chemistry, Jilin University, Changchun, 130023;
    2. Department of Electronic Science, Jilin University
  • Received:1990-12-20 Online:1991-11-24 Published:1991-11-24

Abstract: The precursors of LaFeO3were prepared by cifrnle process and nanocrystals of LaFeO3were synthesized by a solid phase reaction at 400-500℃ for 2 h. The nanocrystalline material of LaFeO3was obtained at 0. 5 GPa. The characterization of the samples was carried out by XRD and TEM. The size of the crystals is about 12. 4 nm by TEM. The diffracted X-ray intensity of the compact sample was attributed to the contribution from the LaFeO3nanocrystals and the interfaces.

Key words: Lanthanum ferrite, Nanocrystalline, Synthesis

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