The Preparation of Co3O4Ultrafine Particles

Chem. J. Chinese Universities ›› 1991, Vol. 12 ›› Issue (11): 1421.

• Articles • Next Articles

The Preparation of Co₃O₄Ultrafine Particles

Wang Xiao-hui, Wang Zi-chen, Li Xi, Xu Bao-kun, Zhao Mu-yu

Department of Chemistry, Jilin University, Changchun, 130023

Received:1990-10-10 Online:1991-11-24 Published:1991-11-24

Abstract

Abstract: Co₃O₄ultrafine particles (UFP) were prepared from CoCl₂by colloidal chemical method. The most favorable experiment conditions for the preparation of Co₃O₄UFP were studied. XRD, DTA, TG, IR and TEM examinations were used to discribe the characteristic of the sample. The spherical amorphous ultrafine Co₃O₄product has average diameters of 4. 0 nm, with good dispersity and transparency in many organic solvents. When heat-treated at 800 Kfor 3 hours, cubic crystal Co₃O₄UFPcan be obtained, the average crystal grain size is 6. 0 nm.

Key words: Is Ultrafine particle, Co₃O₄, Colloidal chemical method

TrendMD:

Wang Xiao-hui, Wang Zi-chen, Li Xi, Xu Bao-kun, Zhao Mu-yu . The Preparation of Co₃O₄Ultrafine Particles[J]. Chem. J. Chinese Universities, 1991, 12(11): 1421.

[1]	JIN Xin, FENG Xilan, LIU Dapeng, SU Yutong, ZHANG Zheng, ZHANG Yu. Auto-redox Strategy for the Synthesis of Co₃O₄/CeO₂ Nanocomposites and Their Structural Optimization Towards Catalytic CO Oxidation [J]. Chem. J. Chinese Universities, 2020, 41(4): 652.
[2]	ZHOU Hai, CHEN Hao, GUO Ya, KANG Min. Synthesis of Meso-porous Co₃O₄ Polyhedra and Their Electrochemical Properties^† [J]. Chem. J. Chinese Universities, 2019, 40(7): 1374.
[3]	ZENG Liangpeng, HUANG Fan, ZHU Xing, ZHENG Min, LI Kongzhai. Chemical Looping Conversion of Methane over CeO₂-based and Co₃O₄-based Co₃O₄-CeO₂ Oxygen Carriers:Controlling of Product Selectivity^† [J]. Chem. J. Chinese Universities, 2017, 38(1): 115.
[4]	ZHANG Ye, ZHOU Jiajia, WU Guisheng, MAO Dongsen, LU Guanzhong. Influence of the Surface Species over Co₃O₄ on the Formaldehyde Catalytic Oxidation Performance^† [J]. Chem. J. Chinese Universities, 2014, 35(12): 2598.
[5]	ZHANG Wei-Min, ZHANG Yu, DONG Guang-Ming, SUN Zhong-Xi. Hydrothermal Synthesis of Polycrystal Co₃O₄ with One Dimensional Nanostructures [J]. Chem. J. Chinese Universities, 2006, 27(10): 1791.
[6]	JIA Ming-Jun, ZHANG Wen-Xiang, TAO Yu-Guo, WANG Gui-Ying, CUI Xiang-Hao, ZHANG Chun-Lei, WU Tong-Hao, DONG Guo-Qiang, LI Xue-Mei. Preparation, Characterization and CO Oxidation of Nanometer Co₃O₄ [J]. Chem. J. Chinese Universities, 1999, 20(4): 637.
[7]	LI Ya-Dong, HE Yun-Pu, LI Long-Quan, QIAN Yi-Tai . Fabrication of Co₃O₄Ultrafines by a Liquid-control-precipitation Method [J]. Chem. J. Chinese Universities, 1999, 20(4): 519.
[8]	WANG Zi-Chen, ZHANG Li-Hua, Li Xi, XU Bao-Kun, ZHAO Mu-Yu . Preparation of Nanocrystalline Materials of NiO by Colloidal-Method [J]. Chem. J. Chinese Universities, 1992, 13(10): 1287.

The Preparation of Co₃O₄Ultrafine Particles

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 8

Recommended Articles

Metrics

Comments