Chem. J. Chinese Universities ›› 2017, Vol. 38 ›› Issue (4): 522.doi: 10.7503/cjcu20160909
• Articles: Inorganic Chemistry • Previous Articles Next Articles
HUANG Run1, PAN Chengling1*1(), ZHANG Lan2
Received:
2016-12-16
Online:
2017-04-10
Published:
2017-03-22
Supported by:
CLC Number:
TrendMD:
HUANG Run, PAN Chengling*, ZHANG Lan. Effect of Surface Mechanical Attrition Treatment on Bioactivity of Biomedical Titanium Alloy†[J]. Chem. J. Chinese Universities, 2017, 38(4): 522.
Element | Ti | Nb | Mo | Sn | Zr | C | N | H | O | Fe |
---|---|---|---|---|---|---|---|---|---|---|
Content/(%, mass ratio) | 66.687 | 25.1 | 2.90 | 2.02 | 3.08 | 0.01 | 0.03 | 0.003 | 0.14 | 0.03 |
Table 1 Chemical composition of TLM titanium alloy
Element | Ti | Nb | Mo | Sn | Zr | C | N | H | O | Fe |
---|---|---|---|---|---|---|---|---|---|---|
Content/(%, mass ratio) | 66.687 | 25.1 | 2.90 | 2.02 | 3.08 | 0.01 | 0.03 | 0.003 | 0.14 | 0.03 |
Ion | Ion concentration/(mmol·L-1) | |
---|---|---|
Blood | SBF | |
Na+ | 142.0 | 142.0 |
K+ | 5.0 | 5.0 |
Mg2+ | 1.5 | 1.5 |
Ca2+ | 2.5 | 2.5 |
Cl- | 103.0 | 147.8 |
HC | 27.0 | 4.2 |
HP | 1.0 | 1.0 |
S | 0.5 | 0.5 |
pH | 7.2—7.4 | 7.40 |
Table 2 Ion concentrations of SBF and human blood plasma[20]
Ion | Ion concentration/(mmol·L-1) | |
---|---|---|
Blood | SBF | |
Na+ | 142.0 | 142.0 |
K+ | 5.0 | 5.0 |
Mg2+ | 1.5 | 1.5 |
Ca2+ | 2.5 | 2.5 |
Cl- | 103.0 | 147.8 |
HC | 27.0 | 4.2 |
HP | 1.0 | 1.0 |
S | 0.5 | 0.5 |
pH | 7.2—7.4 | 7.40 |
Sample | Surface roughness/nm | ||
---|---|---|---|
Ra | Rq | Rz | |
TLM | 14.7±1.5 | 22.9±2.1 | 51.6±3.8 |
SMAT-TLM | 32.6±2.9 | 49.2±3.5 | 98.4±6.8 |
Table 3 Surface roughness of different samples
Sample | Surface roughness/nm | ||
---|---|---|---|
Ra | Rq | Rz | |
TLM | 14.7±1.5 | 22.9±2.1 | 51.6±3.8 |
SMAT-TLM | 32.6±2.9 | 49.2±3.5 | 98.4±6.8 |
Sample | Area percent of O1s peak(%) | ||
---|---|---|---|
530.1 eV | 531.3 eV | 532.8 eV | |
SMAT-TLM | 59.6 | 18.7 | 21.7 |
TLM | 50.4 | 35.5 | 14.1 |
Table 4 Area percent of the O1s peaks at different binding energies
Sample | Area percent of O1s peak(%) | ||
---|---|---|---|
530.1 eV | 531.3 eV | 532.8 eV | |
SMAT-TLM | 59.6 | 18.7 | 21.7 |
TLM | 50.4 | 35.5 | 14.1 |
Fig.6 SEM images of the TLM(A) and SMAT-TLM(B) surfaces after immersed in SBF solution for 28 d The inset in (B) is the magnified image of the white dotted square.
Fig.8 Total protein adsorbed onto TLM and SMAT-TLM surfaces after 1, 4 and 24 h of incubation in DMEMData are presented as the mean±SD, n=5, * P<0.05 compared with the TLM surface.
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