高等学校化学学报

高等学校化学学报 ›› 2005, Vol. 26 ›› Issue (4): 595.

• 研究论文 •    下一篇

铌酸锂多晶粉体的水热合成及表征

吁霁1,2, 刘兴泉1   

  1. 1. 中国科学院成都有机化学研究所, 成都 610041;
    2. 中国科学院研究生院, 北京 100039
  • 收稿日期:2004-09-17 出版日期:2005-04-10 发布日期:2005-04-10
  • 通讯作者: 刘兴泉(1964年出生),男,研究员,主要从事无机功能材料化学研究.E-mail:Lxquan2000@hotmail.com,Lxquan2000@sina.com E-mail:Lxquan2000@hotmail.com;Lxquan2000@sina.com
  • 基金资助:

    中国科学院青年创新基金资助.

Hydrothermal Synthesis and Characterization of LiNbO3 Polycrystal Powder

YU Ji1,2, LIU Xing-Quan1   

  1. 1. Chengdu Institute of Organic Chemistry, Chinese Academy of Sciences, Chengdu 610041, China;
    2. Graduate School of the Chinese Academy of Sciences, Beijing 100039, China
  • Received:2004-09-17 Online:2005-04-10 Published:2005-04-10

PDF (PC)

被引次数

15

摘要： 铌酸锂(LiNbO3)晶体由于本身具有的优良性能在许多领域中都获得了广泛的应用.以LiOH·H2O和Nb2O5为原料采用水热合成法成功地合成了铌酸锂多晶粉体,并采用FTIR谱、XRD谱和SEM对产物进行了表征.结果表明,采用水热合成法能够得到结晶完整的四方柱形LiNbO3多晶粉体.同时考察了反应温度、晶化时间和Li源对水热合成产物的影响.

关键词: 铌酸锂, 水热合成法, 红外光谱, X射线衍射

Abstract: LiNbO3 crystals were widely used in many fields because of their excellent ferric properties. In this work, LiNbO3 powders were successfully prepared via a simple and convenient hydrothermal method with LiOH·H2O and Nb2O5 as the starting materials. FTIR spectra and XRD patterns of the as-prepared samples showed good crystalline and high purity. At the same time, the effects of different Li sources, crystallization temperature and time on the as-prepared product were also investigated.

Key words: LiNbO3, Hydrothermal synthesis method, IR spectra, XRD

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