Simutaneous Determination of 17 Components in Oxidative Hair Dyes by Gas Chromatography-Mass Spectrometry

Chem. J. Chinese Universities ›› 2011, Vol. 32 ›› Issue (10): 2286.

• Preface • Previous Articles Next Articles

Simutaneous Determination of 17 Components in Oxidative Hair Dyes by Gas Chromatography-Mass Spectrometry

LAI Ying*, CHEN He-Xiu, LIN Rui, WANG Hong-Hui, DONG Qing-Mu, HUANG Zong-Ping

Xiamen Entry-Exit Inspection and Quarantine Bureau, Xiamen 361026, China

Received:2010-11-05 Revised:2010-12-21 Online:2011-10-10 Published:2011-09-11
Contact: LAI Ying E-mail:laiy@xmciq.gov.cn
Supported by:
出入境检验检疫行业标准(批准号:2009B101,2009B105)和厦门检验检疫局2007年科技项目(批准号:2007XK03)资助.

Abstract

Abstract: A reliable Gas Chromatography-Mass Spectrometry(GC-MS) method was developed for the simultaneous determination of 17 dye intermediates, including benzenediamines, aminophenols, benzenediols, naphthalenediol and diaminopyridine, in oxidative hair dyes. Samples were extracted with 50% ethanol by adding sodium dithionite to prevent oxidation. A DB-WAX capillary column was selected for the separation of both water soluble and alcohol soluble hair dye intermediates. The results showed that 17 dye intermediates were well separated within 25 min. The detection limits of these compounds were in the range of 2-380 mg/kg. The recoveries of the target compounds in hair dyes ranged from 81.1% to 103.7% with four addition levels. The method described was validated by 5 different laboratories and successfully applied to the analysis of commercial oxidative hair dyes.

Key words: Gas chromatography\, mass spectrometry, Benzenediamine, Aminophenol, Benzenediol, Hair dye

CLC Number:

TrendMD:

LAI Ying*, CHEN He-Xiu, LIN Rui, WANG Hong-Hui, DONG Qing-Mu, HUANG Zong-Ping. Simutaneous Determination of 17 Components in Oxidative Hair Dyes by Gas Chromatography-Mass Spectrometry[J]. Chem. J. Chinese Universities, 2011, 32(10): 2286.

[1]	ZHU Kai, LI Jie, WU Xiaoyi, HU Weiwei, WU Dongmei, YU Chengxiao, GE Zhiwei, YE Xingqian, CHEN Shiguo. Combined PGC-Triple-Tof-MS Enables the Separation， Identification of Sugar Beet Pectin Derived Oligomers [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220023.
[2]	LIANG Quntao, ZOU Qiang, LIN Jianghui, LIU Shutao, WEI Zheng. Ultraviolet Absorbance of Saturated Structure in the Non-reducing End of Heparin/Heparan Sulfate Disaccharides and Its Application in Sequence of Heparin Oligosaccharides [J]. Chem. J. Chinese Universities, 2021, 42(6): 1776.
[3]	DOU Shuzhen, WANG Zhongshun, LYU Nan. Improving the Detection Performance of Surface-assisted Laser Desorption/ionization Mass Spectrometry by Silicon Nanostructures [J]. Chem. J. Chinese Universities, 2021, 42(4): 1156.
[4]	ZHENG Haijiao, JIANG Liyan, JIA Qiong. Arginine Functionalized Magnetic Nanoparticles and Its Application in Phosphopeptides Enrichment [J]. Chem. J. Chinese Universities, 2021, 42(3): 717.
[5]	WANG Ruxin, ZHAO Zhongjun, HE Feiyao, YUE Hanlu, DENG Fulong, LI Hong, LI Wenwen, DUAN Yixiang. Characteristic Analysis of C₁—C₃n-Aldehydes and n-Alcohols in Proton Transfer Reaction Time-of-flight Mass Spectrometry [J]. Chem. J. Chinese Universities, 2021, 42(12): 3632.
[6]	ZHAO Huanhuan, LI Cunyu, JIN Hong. Evaluation of Quantitative Phosphoproteomic Performance of Sequential Enrichment of Metal Oxide Affinity Chromatography for Phosphopeptides Using TMT 10-plex Isobaric Labeling [J]. Chem. J. Chinese Universities, 2021, 42(12): 3624.
[7]	WANG Baichun, YUAN Yuxin, YAN Yinghua, DING Chuanfan, TANG Keqi. Glucose-6-phosphate Functionalized Hydrophilic Magnetic Probe： a Dual-purpose Affinity Material for Effective Separation and Enrichment of Glycopeptides/Phosphopeptides [J]. Chem. J. Chinese Universities, 2021, 42(10): 3062.
[8]	DENG Jiewei, YANG Yunyun, LIN Li, LUAN Tiangang. Rapid Classification of Daphniamagna and Daphnia pulex by Surface-coated Probe Nanoelectrospray Ionization Mass Spectrometry Lipidomics [J]. Chem. J. Chinese Universities, 2020, 41(9): 2011.
[9]	LI Xiaoqian, ZHANG Hua, LU Haijian, LIU Chang, LIU Qinglong, MA Xiayu, FANG Yuanping, LIANG Dapeng. Mechanism of Photocatalytic Degradation of Rhodamine B by TiO₂ Nanowire Array with Internal Extraction Electrospray Ionization Mass Spectrometry [J]. Chem. J. Chinese Universities, 2020, 41(9): 2003.
[10]	WANG Xiaoyu, YAN Guoquan, ZHOU Xinwen, YANG Pengyuan. Assignment of Polypeptide Disulfide Bonds by Chemical Cleavage and Bio-mass Spectrometry^† [J]. Chem. J. Chinese Universities, 2020, 41(7): 1505.
[11]	HE Yu, XIA Qian, WANG Wenli, LUO Fang, CHEN Jinfeng, GUO Yating, WANG Jian, LIN Zhenyu, CHEN Guonan. Triglycerides as Potential Biomarkers for Pesticides Pollution in Aquatic Environment Using UPLC-QTOF-MS ^† [J]. Chem. J. Chinese Universities, 2020, 41(3): 431.
[12]	WANG Tianqi,YU Qiongwei,FENG Yuqi. Analysis of Imidazole Propionic Acid in Serum of Patients with Type 2 Diabetes Based on NiO@SiO₂ Solid-phase Extraction Coupled with Liquid Chromatography-Mass Spectrometry ^† [J]. Chem. J. Chinese Universities, 2020, 41(2): 262.
[13]	WANG Xiaoqun, HUANG Guangming. Investigation of Lipid Distributions by Trifluoroacetic Acid-enhanced Desorption Electrospray Ionization Mass Spectrometry Imaging [J]. Chem. J. Chinese Universities, 2020, 41(12): 2673.
[14]	AI Wanpeng, SONG Shiyao, BAI Yu, LIU Huwei. Development and Applications of Mass Spectrometry in Reaction Monitoring [J]. Chem. J. Chinese Universities, 2020, 41(12): 2598.
[15]	WANG Lianping,LI Qingjie,LIU Xiaoyan,REN Yueying,YANG Xiuwei. Screening of Cholinesterase Inhibitors in Fructus Evodiae Alkaloids Based on UFLC-MS/molecular Simulation ^† [J]. Chem. J. Chinese Universities, 2020, 41(1): 111.

Simutaneous Determination of 17 Components in Oxidative Hair Dyes by Gas Chromatography-Mass Spectrometry

PDF (PC)

Knowledge

Cited

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments