Preparation of Interpenetrating Network Polyvinyl Alcohol Composite Coatings for Solid-phase Microextraction

doi:10.7503/cjcu20120680

Chem. J. Chinese Universities ›› 2013, Vol. 34 ›› Issue (3): 698.doi: 10.7503/cjcu20120680

• Polymer Chemistry • Previous Articles Next Articles

Preparation of Interpenetrating Network Polyvinyl Alcohol Composite Coatings for Solid-phase Microextraction

ZHANG Meng-Juan¹, FEI Xu², TIAN Jing³, FAN Shu-Qi¹, WANG Yi³

1. School of Textile and Material Engineering, Dalian Polytechnic University, Dalian 116034, China;
2. Modern Education Technical Department, Dalian Polytechnic University, Dalian 116034, China;
3. School of Biological Engineering, Dalian Polytechnic University, Dalian 116034, China

Received:2012-07-18 Online:2013-03-10 Published:2013-02-18

Abstract

Abstract:

PVA/SiO₂ composite coatings which have the interpenetrating organic and inorganic cross-linked network were prepared by repeated freezing-thawing and sol-gel techniques. The structure and characterization of the composite membrane were determined by FTIR, TGA, SEM and gas chromatography. The composite coatings have good thermal stability(T_d>300 ℃) and good adherence activity that they are difficult shedding from coated glass or quartz fiber surface by chemical bonds. The performance of the coatings was tested by extraction of 1-propanol, 1- butanol, amyl alcohol and toluene. The fiber coatings proved to be selective for polar compounds containing hydroxyl groups. The relative standard deviation(RSD, n=3) was less than 5%.

Key words: Poly(vinyl alcohol), Sol-gel method, Freezing-thawing, Solid-phase microextraction

CLC Number:

O635

TrendMD:

ZHANG Meng-Juan, FEI Xu, TIAN Jing, FAN Shu-Qi, WANG Yi. Preparation of Interpenetrating Network Polyvinyl Alcohol Composite Coatings for Solid-phase Microextraction[J]. Chem. J. Chinese Universities, 2013, 34(3): 698.

References

Related Articles 15

[1]	JIANG Xiaokang, ZHOU Qi, ZHOU Hengwei. Synthesis and Luminescence Properties of Gd₂ZnTiO₆∶Dy³⁺， Eu³⁺ Single Phase White Light-emitting Phosphors [J]. Chem. J. Chinese Universities, 2022, 43(6): 20220029.
[2]	ZHANG Yong, XU Jun, BAO Yu, CUI Shuxun. Quantifying the Degree of Weakening Effect of Nonpolar Organic Solvent on the Strength of Intramolecular Hydrogen Bonding by Single-molecule Force Spectroscopy [J]. Chem. J. Chinese Universities, 2022, 43(4): 20210863.
[3]	BAI Jingqi, BAI Shan, REN Lixia, ZHU Kongying, ZHAO Yunhui, LI Xiaohui, YUAN Xiaoyan. Trehalose-modified Poly（vinyl alcohol） and Their Antifogging/Antifrosting Coatings [J]. Chem. J. Chinese Universities, 2021, 42(8): 2683.
[4]	LI Yishan, GUO Liang, PENG Sifan, ZHANG Qingmao, ZHANG Yuhao, XU Shiqi. Cobalt Substitutions in Lanthanum Manganate Photocatalyst： First-principles and Visible-light Photocatalytic Ability Investigation [J]. Chem. J. Chinese Universities, 2021, 42(6): 1881.
[5]	HAN Yandong, HAN Mingyong, YANG Wensheng. Sol-gel Construction of Mesoporous Silica Nanomicrostructures [J]. Chem. J. Chinese Universities, 2021, 42(4): 965.
[6]	WANG Jie, LI Ying, SHAO Liang, BAI Yang, MA Zhonglei, MA Jianzhong. Preparation and Properties of Poly（vinyl alcohol）/polypyrrole Composite Conductive Hydrogel Strain Sensor [J]. Chem. J. Chinese Universities, 2021, 42(3): 929.
[7]	DENG Jiewei, YANG Yunyun, LIN Li, LUAN Tiangang. Rapid Classification of Daphniamagna and Daphnia pulex by Surface-coated Probe Nanoelectrospray Ionization Mass Spectrometry Lipidomics [J]. Chem. J. Chinese Universities, 2020, 41(9): 2011.
[8]	HAN Hongjing,GE Qin,CHEN Yanguang,WANG Haiying,ZHAO Hongzhi,WANG Yizhen,ZHANG Yanan,DENG Jitong,SONG Hua,ZHANG Mei. Production of Phenolic Compounds from Bagasse Lignin via Catalytic Pyrolysis of Ca₁_-xPr_xFe $O 3 †$ [J]. Chem. J. Chinese Universities, 2020, 41(2): 331.
[9]	REN Chenrui, LIU Genqi, QIN Xiatong, LIU Chenhui, FAN Xiaodong. Preparation of PVA Two-dimensional Photonic Crystal Hydrogel and Its Responsive Behavior to Ethanol^† [J]. Chem. J. Chinese Universities, 2019, 40(7): 1520.
[10]	ZHANG Shuming, LUO Jianhui, XIA Bibo, LI Yuanyang, HE Meiying, JIANG Bo. Sol-gel Preparation of Superhydrophilic Silica Coating-materials with Low Refractive Index^† [J]. Chem. J. Chinese Universities, 2018, 39(6): 1342.
[11]	LUO Jianhui,YANG Jie,LI Yuanyang,HE Lipeng,JIANG Bo. Synthesis of Amphiphilic Silica Nanoparticles with Double-sphere Morphology^† [J]. Chem. J. Chinese Universities, 2018, 39(10): 2170.
[12]	YANG Tao, CHENG Tiexin, ZHOU Guangdong. Effects of Ag or Yb Doping on Thermoelectric Properties of Ca₃Co_3.9Cu_0.1 $O 9 - δ †$ [J]. Chem. J. Chinese Universities, 2017, 38(3): 335.
[13]	HE Meiying, LUO Jianhui, YANG Bowen, XIA Bibo, LI Yuanyang, ZHANG Shuming, JIANG Bo. Sol-gel Preparation of Hydrophobic Silica Coating-materials with Ultralow Refractive Index^† [J]. Chem. J. Chinese Universities, 2017, 38(11): 2077.
[14]	XIA Yanyang, BU Tiantong, WANG Licheng, ZHU Wanchun, YANG Xuwei, BAO Qiang, HAO Mengmeng, CHENG Dongdong, WANG Zhenlü. Hydrodealkylation of Trimethylbenzene over Silicon-based Catalyst^† [J]. Chem. J. Chinese Universities, 2016, 37(12): 2215.
[15]	YIN Hong, ZHOU Dan, CONG Lina, XIE Haiming, QIU Yongqing. MoO₂/C Co-coated Si/graphite Composite as Anode Materials for Lithium Ion Batteries^† [J]. Chem. J. Chinese Universities, 2015, 36(10): 1990.

Preparation of Interpenetrating Network Polyvinyl Alcohol Composite Coatings for Solid-phase Microextraction

PDF (PC)

Knowledge

Cited

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments