Chem. J. Chinese Universities ›› 2010, Vol. 31 ›› Issue (9): 1721.

• Articles • Previous Articles     Next Articles

Homogeneous Ionic Liquid Microextraction of Fleroxacin and Sulfaquinoxaline from Water Samples

WANG Ying, XIAO Yao, REN Rui-Bing, BAO Chang-Li, ZHANG Han-Qi, YU Ai-Min, WANG Ying-Hua*   

  1. College of Chemistry, Jilin University, Changchun 130012, China
  • Received:2010-03-29 Online:2010-09-10 Published:2010-09-10
  • Contact: WANG Ying-Hua. E-mail: jl.wyh@163.com
  • Supported by:

    质检公益性行业科研专项经费(批准号: 200810474)资助.

Abstract: The homogeneous liquid microextraction was developed for extracting fleroxacin and sulfaquinoxaline from water samples. A room temperature ionic liquid [C6MIm][BF4], which is dissolvable in water, and NH4PF6, can be sequentially added into the water samples. The resulting [C6MIm] [PF6], which is not dissolvable in water, can be dispersed in the sample solution as very fine drops. After extraction, phase separation was performed by centrifugation. The sedimented phase was taken with a high performance liquid chromatography(HPLC) microsyringe and injected into the HPLC system for analysis. The detection limits for fleroxacin and sulfaquinoxaline were found to be 1.8 and 1.1 μg/L, respectively.

Key words: Lonic liquid, Homogeneous liquid microextraction, High performance liquid chromatography(HPLC)

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