Chem. J. Chinese Universities
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LIU Gui-Yan1, MA Shuang-Cheng2, ZHENG Jian2, YU Zhen-Xi2, LIN Rui-Chao2
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Abstract: To study the chemical constituents, the ethanol extract of dried stem of Akebia quinata(Thunb.) Decne. was seperated by dichloromethane, n-butanol in sequence. The n-butanol extract was further isolated by D101 macroporous resin and silica gel column chromatography. A new triterpene with two known triterpenes were isolated, their structures were identified as 3α,24-dihydroxy-30-norolean-12,20(29)-dien-28-oic acid (Ⅰ), 3α,24,29-trihydroxyolean-12-en-28-oic acid (Ⅱ), 2α,3β,23-trihydroxyolean-12-en-28-oic acid (Ⅲ). The new compound Ⅱ was nominated as quinatic stem acid. The structures were identified and elucidated by physicochemical properties and spectral analysis.
Key words: Akebia, Akebia quinata(Thunb.)Decne., Triterpene, Quinatic stem acid
CLC Number:
O625
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LIU Gui-Yan1, MA Shuang-Cheng2, ZHENG Jian2, YU Zhen-Xi2, LIN Rui-Chao2. A New Triterpene from Akebia Quinata Stem[J]. Chem. J. Chinese Universities, doi: .
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URL: http://www.cjcu.jlu.edu.cn/EN/
http://www.cjcu.jlu.edu.cn/EN/Y2006/V27/I11/2120