Chem. J. Chinese Universities ›› 2003, Vol. 24 ›› Issue (4): 651.
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ZHANG Tian Zhu, XU Li Jin, CHEN Yong, MO Jun, SUN Wen Hua
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Abstract: A more convenient and economic method has been developed for synthesizing bis (4 bromophenyl)phosphine oxide in a high yield, which was introduced to prepare three water soluble phosphine precursors successfully. All new compounds were fully characterized by IR, 1HNMR, 13CNMR, 31PNMR, MALDI TOFMS and elemental analyses.
Key words: Grignard reaction, Organic phosphine, Water soluble phosphine compound
CLC Number:
O641
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ZHANG Tian Zhu, XU Li Jin, CHEN Yong, MO Jun, SUN Wen Hua. Novel Synthesis of Bis(4-bromophenyl)phosphine Oxide and Its Application in the Preparation of Water-soluble Phosphine Precursors[J]. Chem. J. Chinese Universities, 2003, 24(4): 651.
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http://www.cjcu.jlu.edu.cn/EN/Y2003/V24/I4/651