Synthesis, Characterization and Catalysis Acitivity of the MCM-48 Framework Containing Ti, Co, Cr, Mn, Cu, Mo

Chem. J. Chinese Universities ›› 1999, Vol. 20 ›› Issue (3): 344.

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Synthesis, Characterization and Catalysis Acitivity of the MCM-48 Framework Containing Ti, Co, Cr, Mn, Cu, Mo

CAI Qiang¹, WEI Chang-Ping², XU Yong-Yi¹, PANG Wen-Qin¹, ZHEN Kai-Ji²

1. The Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun, 130023;
2. the Laboratory of Catalysis of Department of Chemistry, Jilin University, Changchun, 130023

Received:1998-03-27 Online:1999-03-24 Published:1999-03-24

Abstract

Abstract: In this paper, the MCM-48 framework containing Ti, Co, Zr, Cr, Mn, Cu and Mo was synthesized and characterized by means of HRTEM, pore diameter distribution, XRD, XPS and IR absorption spectra. In addition, we also studied their catalysis behavior for the conversion from eicosanol to eicosanic acid. The experimental results show that the Ti, Cr, Zr doped MCM-48 pocesses excellent catalysis properties.

Key words: Mesoporous molecular sieve MCM-48, Transition metal, IR spectra, Electron energy spectrum, Eicosanol

CLC Number:

O614

TrendMD:

CAI Qiang, WEI Chang-Ping, XU Yong-Yi, PANG Wen-Qin, ZHEN Kai-Ji . Synthesis, Characterization and Catalysis Acitivity of the MCM-48 Framework Containing Ti, Co, Cr, Mn, Cu, Mo[J]. Chem. J. Chinese Universities, 1999, 20(3): 344.

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Synthesis, Characterization and Catalysis Acitivity of the MCM-48 Framework Containing Ti, Co, Cr, Mn, Cu, Mo

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