Chem. J. Chinese Universities ›› 1997, Vol. 18 ›› Issue (6): 902.

• Articles • Previous Articles     Next Articles

Synthesis and Structure of 1-(m-Methoxyphenyl)-2-(dimethylaminomethyl) cyclohexanol

QIAO Ben-Zhi, JIN Chun, SUN Wen-Yang   

  1. Department of Applied Chemistry, Taiyuan University of Technology, Taiyuan, 030024
  • Received:1996-08-08 Online:1997-06-24 Published:1997-06-24

Abstract: The reaction of 2-(dimethylaminomethyl) cyclohexanone with m-anisyl magne-sium bromlde yielded the title compound as a mixture of Z- and E-isomers, which were sepa-rated into their pure component by fractional crystallization. Their configurations were de-termined by 13CNMRspectra. The stereochemistry of the reaction was discussed.

Key words: 1-(m-Methoxyphenyl)-2-(dimethylaminomethyl)-cyclohexanol, Synthesis, Separation, Structure

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